缬沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数4000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.131194631191061194201192071192661192920.13
214.101174541178131176340.22
单位质量响应值RSD%判断
8442.468342.840.84数据可信
供试品溶液-8194970批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1184752-18475269.49765.867.1669.5065.867.16
2182868-18286868.78868.79
3175726-17572666.10266.10
4161883-16188360.89460.89
5157758-15775859.34359.34
6187590-18759070.56570.56
10min1237464-23746489.32587.335.7789.4487.445.77
2247885-24788593.24593.36
3237151-23715189.20889.32
4218561-21856182.21582.32
5213042-21304280.13980.24
6238810-23881089.83289.95
15min1251470-25147094.59492.624.9194.8692.874.92
2258724-25872497.32397.59
3249357-24935793.79994.06
4236980-23698089.14389.38
5226555-22655585.22285.45
6254200-25420095.62195.89
20min1258386-25838697.19594.894.2797.6295.304.28
2261038-26103898.19398.63
3258106-25810697.09097.51
4238206-23820689.60489.99
5238635-23863589.76690.14
6259205-25920597.50397.93
30min1262661-26266198.80497.352.1599.3997.922.17
2260845-26084598.12098.72
3261886-26188698.51299.09
4251816-25181694.72495.26
5251658-25165894.66595.19
6263873-26387399.25999.85
45min1260607-26060798.03197.541.1798.7898.281.18
2256735-25673596.57497.33
3264341-26434199.435100.18
4256815-25681596.60497.30
5257073-25707396.70297.38
6260314-26031497.92198.68
60min1260100-26010097.84098.070.9398.7598.960.92
2257763-25776396.96197.88
3264535-26453599.508100.42
4258834-25883497.36498.22
5261057-26105798.20099.04
6261937-26193798.53199.45
90min1261652-26165298.42498.380.9799.5099.440.95
2256907-25690796.63997.72
3264006-26400699.309100.38
4262205-26220598.63299.65
5261061-26106198.20299.21
6263389-26338999.077100.16
120min1257654-25765496.92096.041.3398.1697.261.34
2254007-25400795.54896.79
3256645-25664596.54197.78
4250049-25004994.05995.24
5253959-25395995.53096.70
6259639-25963997.66798.91
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1258138-25813897.10295.931.5998.5097.311.60
2252950-25295095.15196.55
3257741-25774196.95398.35
4249379-24937993.80795.15
5252282-25228294.89996.23
6259621-25962197.66099.07
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