叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.379097191058910749114391173910840.09
210.379105791080910680.02
单位质量响应值RSD%判断
8783.418781.870.02数据可信
供试品溶液-21FA624批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1103707-10370796.92293.524.2596.9293.524.25
2100145-10014593.59393.59
397317-9731790.95090.95
4106470-10647099.50499.50
597243-9724390.88090.88
695543-9554389.29289.29
10min1112363-112363105.011100.395.45105.17100.545.45
2109579-109579102.409102.57
3100693-10069394.10594.26
4115166-115166107.631107.80
5104695-10469597.84598.00
6101984-10198495.31195.46
15min1108882-108882101.75898.294.97102.0998.624.97
2103214-10321496.46196.79
3104123-10412397.31097.62
4113701-113701106.262106.61
599474-9947492.96593.28
6101655-10165595.00495.31
20min1108700-108700101.58898.654.17102.0999.144.17
2108117-108117101.043101.53
3102518-10251895.81096.28
4111347-111347104.062104.58
5102238-10223895.54996.02
6100433-10043393.86294.33
30min1108620-108620101.51398.823.78102.1999.473.78
2107422-107422100.393101.05
3101966-10196695.29495.92
4111293-111293104.011104.71
5103759-10375996.97097.60
6101340-10134094.70995.33
45min1108330-108330101.24297.993.50102.0998.813.50
2105669-10566998.75599.58
3101979-10197995.30796.10
4109454-109454102.293103.16
5103672-10367296.88997.68
6100014-10001493.47094.25
极限1108088-108088101.01697.694.12102.0398.674.12
2105064-10506498.19099.18
3101898-10189895.23196.18
4110856-110856103.603104.64
5101689-10168995.03695.99
699589-9958993.07394.01
叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.379099391169911129113291066910940.08
210.379107091015910420.05
单位质量响应值RSD%判断
8784.388779.360.05数据可信
供试品溶液-21FA624批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min199216-9921692.73393.261.9992.7393.261.99
298927-9892792.46292.46
3102697-10269795.98695.99
497873-9787391.47791.48
5101769-10176995.11995.12
698216-9821691.79891.80
10min1103955-10395597.16299.693.1297.3299.843.12
2104459-10445997.63397.79
3111460-111460104.176104.34
4106954-10695499.965100.12
5109707-109707102.538102.70
6103405-10340596.64896.80
15min1103006-10300696.27598.703.2396.5999.023.23
2104160-10416097.35397.67
3110517-110517103.295103.63
4103160-10316096.41996.74
5109363-109363102.216102.55
6103407-10340796.65096.96
20min1103240-10324096.49498.523.2096.9799.003.20
2104075-10407597.27497.75
3109761-109761102.588103.09
4103202-10320296.45896.94
5109655-109655102.489102.99
6102490-10249095.79396.27
30min1103032-10303296.29997.982.5096.9498.632.50
2103594-10359496.82497.47
3107291-107291100.280100.96
4103158-10315896.41797.06
5108966-108966101.845102.52
6102944-10294496.21796.85
45min1102661-10266195.95298.182.8796.7598.992.86
2103312-10331296.56197.36
3107451-107451100.429101.27
4102995-10299596.26597.07
5110037-110037102.846103.69
6103795-10379597.01297.81
极限1102341-10234195.65397.212.3396.6198.192.34
2102859-10285996.13797.10
3107156-107156100.154101.16
4102309-10230995.62396.59
5107081-107081100.084101.10
6102283-10228395.59996.56
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