叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.372278022277642278102277532278772278010.03
210.372271542272802272170.04
单位质量响应值RSD%判断
21967.3121910.990.19数据可信
供试品溶液-AM221354批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1275531-275531103.083102.761.06103.08102.761.06
2277896-277896103.968103.97
3276283-276283103.365103.36
4276133-276133103.309103.31
5270790-270790101.310101.31
6271362-271362101.524101.52
10min1272454-272454101.932101.721.10102.10101.891.10
2273650-273650102.380102.55
3275546-275546103.089103.26
4272801-272801102.062102.23
5267217-26721799.973100.14
6269662-269662100.888101.06
15min1270897-270897101.350101.661.41101.69102.001.41
2272879-272879102.091102.44
3277855-277855103.953104.30
4273175-273175102.202102.54
5268122-268122100.311100.65
6267493-267493100.076100.41
20min1270729-270729101.287100.991.28101.80101.501.28
2271892-271892101.722102.24
3274152-274152102.567103.08
4271215-271215101.469101.98
5266489-26648999.701100.20
6265086-26508699.17699.68
30min1269732-269732100.914100.911.15101.59101.591.15
2271919-271919101.732102.42
3273442-273442102.302102.99
4271150-271150101.444102.13
5266536-26653699.718100.39
6265609-26560999.371100.04
45min1269721-269721100.91099.741.90101.76100.581.89
2261663-26166397.89598.75
3272912-272912102.104102.96
4270334-270334101.139101.99
5260769-26076997.56198.40
6264119-26411998.81499.65
极限1268390-268390100.412100.381.12101.43101.391.12
2270439-270439101.178102.19
3271869-271869101.713102.74
4269542-269542100.843101.86
5265585-26558599.362100.36
6263999-26399998.76999.77
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