叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.372255652257302256882266032267492260670.25
210.372273792272392273090.05
单位质量响应值RSD%判断
21800.1021919.860.39数据可信
供试品溶液-AM221354批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1266107-26610799.91999.021.5699.9299.021.56
2260245-26024597.71897.72
3264208-26420899.20699.21
4262319-26231998.49698.50
5270298-270298101.492101.49
6259109-25910997.29197.29
10min1271225-271225101.841100.451.72102.01100.621.72
2268461-268461100.803100.97
3261535-26153598.20298.37
4264376-26437699.26999.43
5273946-273946102.862103.03
6265620-26562099.73699.90
15min1269606-269606101.23399.701.87101.57100.031.87
2261050-26105098.02098.35
3261777-26177798.29398.62
4263518-26351898.94799.28
5273566-273566102.720103.06
6263599-26359998.97799.31
20min1269165-269165101.067100.021.62101.57100.521.62
2260918-26091897.97098.46
3265901-26590199.841100.33
4263656-26365698.99899.49
5273194-273194102.580103.09
6265464-26546499.677100.17
30min1269646-269646101.24899.631.91101.92100.291.90
2257595-25759596.72397.38
3265209-26520999.582100.24
4262685-26268598.63499.29
5271810-271810102.060102.74
6265037-26503799.517100.18
45min1268246-268246100.72299.671.61101.56100.501.61
2259835-25983597.56498.38
3265064-26506499.527100.35
4263018-26301898.75999.58
5272121-272121102.177103.03
6264414-26441499.283100.11
极限1267639-267639100.49499.391.78101.50100.381.78
2259058-25905897.27298.25
3265355-26535599.636100.63
4261466-26146698.17699.16
5272062-272062102.155103.18
6262545-26254598.58199.57
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