褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)4供试品稀释倍数4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.926453664324645386455264462644820.15
29.976478764710647480.09
单位质量响应值RSD%判断
6500.206494.280.07数据可信
供试品溶液-2025040121批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168797-6879795.20395.500.4295.2095.500.42
269316-6931695.92195.92
368609-6860994.94294.94
469190-6919095.74695.75
569259-6925995.84295.84
668904-6890495.35195.35
10min170206-7020697.15296.311.1698.2197.371.15
270378-7037897.39098.46
368414-6841494.67395.73
469720-6972096.48097.54
570060-7006096.95098.02
668803-6880395.21196.27
15min168799-6879995.20594.611.9997.3496.741.96
269594-6959496.30598.45
366419-6641991.91294.02
469212-6921295.77797.91
569284-6928495.87698.02
666906-6690692.58694.70
20min168234-6823494.42394.351.0897.6297.541.05
268866-6886695.29898.52
367347-6734793.19696.32
467240-6724093.04896.25
568539-6853994.84698.05
668875-6887595.31098.46
30min167667-6766793.63993.321.2097.8897.551.15
266705-6670592.30896.58
367851-6785193.89398.06
467518-6751893.43397.67
568554-6855494.86699.13
666334-6633491.79496.00
极限166759-6675992.38291.501.2797.6796.761.19
266554-6655492.09997.40
367211-6721193.00898.21
465703-6570390.92196.19
565174-6517490.18995.50
665312-6531290.38095.60
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)4供试品稀释倍数4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.926460064504647236445964594645760.16
29.976453464505645200.04
单位质量响应值RSD%判断
6509.686471.410.42数据可信
供试品溶液-2025040121批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168228-6822894.51394.041.6494.5194.041.65
269068-6906895.67795.68
366308-6630891.85491.85
468473-6847394.85394.85
566692-6669292.38692.39
668534-6853494.93794.94
10min169322-6932296.02996.451.4297.0897.491.40
269446-6944696.20197.26
368996-6899695.57796.60
471068-7106898.44799.50
570491-7049197.64898.67
668413-6841394.77095.82
15min168218-6821894.50095.691.0896.6297.801.07
269606-6960696.42298.55
368559-6855994.97297.05
470041-7004197.02599.17
569536-6953696.32598.44
668497-6849794.88696.99
20min167996-6799694.19293.021.4997.3696.201.44
268460-6846094.83598.04
366892-6689292.66395.80
466453-6645392.05595.28
565762-6576291.09794.28
667355-6735593.30496.47
30min168137-6813794.38792.921.4798.6097.141.39
265207-6520790.32894.59
367467-6746793.45997.63
467308-6730893.23997.49
567162-6716293.03797.23
667193-6719393.08097.28
极限164672-6467289.58790.723.2294.8595.963.02
266451-6645192.05297.31
366950-6695092.74397.95
461597-6159785.32890.61
567199-6719993.08898.32
666055-6605591.50396.74
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