叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389093290928909399091890872909180.03
210.389101391061910370.04
单位质量响应值RSD%判断
8758.968770.420.10数据可信
供试品溶液-21FA624批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14771-47718.9367.4749.098.947.4749.09
24585-45858.5888.59
34896-48969.1709.17
44920-49209.2159.22
54754-47548.9048.90
6-0.0000.00
10min18072-807215.11915.284.3915.2215.374.59
28468-846815.86015.96
38323-832315.58915.69
48524-852415.96516.07
58002-800214.98815.09
67566-756614.17114.17
15min110558-1055819.77520.593.2420.0420.843.36
211261-1126121.09221.36
311257-1125721.08421.36
411341-1134121.24121.52
510965-1096520.53720.80
610570-1057019.79719.95
20min112802-1280223.97825.042.3124.4625.522.33
213612-1361225.49526.00
313613-1361325.49726.01
413370-1337025.04225.56
513530-1353025.34125.83
613284-1328424.88125.26
30min115733-1573329.46731.603.4330.2232.363.34
217142-1714232.10632.90
317167-1716732.15332.95
416822-1682231.50732.30
517088-1708832.00532.78
617280-1728032.36533.02
45min119650-1965036.80438.513.7637.8839.623.60
220344-2034438.10439.25
320934-2093439.20940.36
419830-1983037.14138.29
520904-2090439.15340.28
621705-2170540.65341.67
60min121946-2194641.10443.865.4942.5945.405.30
223589-2358944.18145.75
323648-2364844.29245.88
421860-2186040.94342.50
524460-2446045.81347.38
624994-2499446.81348.28
90min124728-2472846.31549.464.9048.2651.494.76
226166-2616649.00851.07
326960-2696050.49552.57
425151-2515147.10749.12
527454-2745451.42153.50
627992-2799252.42854.41
极限126713-2671350.03352.533.3352.4955.113.26
227900-2790052.25654.86
328171-2817152.76355.40
427461-2746151.43453.97
528627-2862753.61856.26
629412-2941255.08857.66
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389131191263914799142091505913960.12
210.389073290790907610.05
单位质量响应值RSD%判断
8805.018743.830.50数据可信
供试品溶液-21FA624批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min116110-1611030.14029.655.1430.1429.655.13
216433-1643330.74530.74
316238-1623830.38030.38
415633-1563329.24829.25
514292-1429226.73926.74
616372-1637230.63130.63
10min125553-2555347.80749.114.1548.1449.444.16
226897-2689750.32250.66
326814-2681450.16750.50
426101-2610148.83349.16
524543-2454345.91846.21
627579-2757951.59851.94
15min131396-3139658.73959.452.6759.6160.322.69
232265-3226560.36561.27
331912-3191259.70560.60
431600-3160059.12159.99
530483-3048357.03157.84
632991-3299161.72362.64
20min134546-3454664.63365.391.9166.1566.931.94
235411-3541166.25167.82
334624-3462464.77966.34
435059-3505965.59267.12
534104-3410463.80665.25
635959-3595967.27668.88
30min137484-3748470.12971.943.0372.3774.203.02
239356-3935673.63275.94
338175-3817571.42273.70
438992-3899272.95175.20
536827-3682768.90071.05
639872-3987274.59776.94
45min140179-4017975.17276.663.2678.1979.723.24
241797-4179778.19981.32
340601-4060175.96179.03
441437-4143777.52580.59
539016-3901672.99675.91
642815-4281580.10383.28
60min141089-4108976.87478.692.9580.7382.612.94
242826-4282680.12484.12
341426-4142677.50581.42
442660-4266079.81383.74
540548-4054875.86279.59
643816-4381681.97686.04
90min142208-4220878.96881.323.2883.6786.113.25
244067-4406782.44687.33
342996-4299680.44285.22
444255-4425582.79787.61
541729-4172978.07182.64
645539-4553985.20090.18
极限142621-4262179.74082.643.4885.3288.333.45
244940-4494084.07989.88
344229-4422982.74988.42
444687-4468783.60689.34
542203-4220378.95884.40
646331-4633186.68192.60
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