叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389161490815914469141391600913780.36
210.389187691900918880.02
单位质量响应值RSD%判断
8803.288852.410.40数据可信
供试品溶液-21FA624批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14699-46998.7382.72155.548.742.72155.54
24062-40627.5547.55
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min17412-741213.78314.043.7713.8814.073.58
27250-725013.48213.57
38072-807215.01115.01
47423-742313.80413.80
57627-762714.18314.18
67519-751913.98213.98
15min110976-1097620.41119.622.4920.6619.802.65
210618-1061819.74519.98
310576-1057619.66719.83
410580-1058019.67419.83
510338-1033819.22419.38
610217-1021718.99919.15
20min112914-1291424.01523.993.6924.4924.393.58
212526-1252623.29323.75
312954-1295424.08924.47
412605-1260523.44023.81
513799-1379925.66026.03
612598-1259823.42723.79
30min116292-1629230.29630.351.2931.0431.021.23
216127-1612729.99030.70
316699-1669931.05331.71
416258-1625830.23330.87
516152-1615230.03630.69
616408-1640830.51231.14
45min118993-1899335.31936.642.8236.4037.652.67
219272-1927235.83836.88
320316-2031637.77938.78
419404-1940436.08337.05
520261-2026137.67738.67
619969-1996937.13438.10
60min121694-2169440.34241.473.5241.8142.883.35
221467-2146739.92041.36
322166-2216641.22042.64
422011-2201140.93142.30
522943-2294342.66444.07
623524-2352443.74545.12
90min124939-2493946.37649.073.6548.3050.943.48
225603-2560347.61149.50
326676-2667649.60651.48
426433-2643349.15450.98
527223-2722350.62352.51
627447-2744751.04052.90
极限127836-2783651.76351.202.1854.2053.622.12
227683-2768351.47953.89
327051-2705150.30452.73
426600-2660049.46551.84
528249-2824952.53154.98
627786-2778651.67054.10
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389160491669917429218491691917780.26
210.389185291246915490.47
单位质量响应值RSD%判断
8841.818819.750.18数据可信
供试品溶液-21FA624批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min114849-1484927.60427.791.4027.6027.791.40
214914-1491427.72427.72
314944-1494427.78027.78
415039-1503927.95727.96
515294-1529428.43128.43
614670-1467027.27127.27
10min125283-2528347.00047.051.7247.3147.361.71
225515-2551547.43147.74
324870-2487046.23246.54
425960-2596048.25848.57
525443-2544347.29747.61
624796-2479646.09546.40
15min130700-3070057.07057.541.9357.9058.381.92
231241-3124158.07658.91
330890-3089057.42358.25
431939-3193959.37360.22
530800-3080057.25658.10
630156-3015656.05956.87
20min134015-3401563.23263.681.4264.7065.161.42
234436-3443664.01565.50
334124-3412463.43564.90
435162-3516265.36566.87
533947-3394763.10664.58
633858-3385862.94164.38
30min137552-3755269.80770.161.4271.9772.341.42
238124-3812470.87173.06
337958-3795870.56272.73
438436-3843671.45173.68
537446-3744669.61071.79
636944-3694468.67770.81
45min139785-3978573.95975.191.2076.9078.141.20
240887-4088776.00778.99
340607-4060775.48778.44
441022-4102276.25879.28
540335-4033574.98177.93
640041-4004174.43477.33
60min141080-4108076.36677.041.7480.1380.831.71
242027-4202778.12681.95
341944-4194477.97281.76
442251-4225178.54382.42
540554-4055475.38879.17
640789-4078975.82579.55
90min141754-4175477.61979.611.4682.2384.261.42
242937-4293779.81884.51
342741-4274179.45484.11
443681-4368181.20185.95
542997-4299779.92984.55
642848-4284879.65384.22
极限142239-4223978.52079.511.3983.9985.041.38
243457-4345780.78586.36
342634-4263479.25584.79
443444-4344480.76086.41
542805-4280579.57385.08
642043-4204378.15683.61
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