玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111000931000191001971000371005421001780.22
211.121002171002061002120.01
单位质量响应值RSD%判断
9016.929011.870.04数据可信
供试品溶液-2025090921批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min158495-5849558.26754.119.9858.2754.129.98
253064-5306452.85752.86
359562-5956259.33059.33
448755-4875548.56548.57
558789-5878958.56058.56
647288-4728847.10447.10
10min174923-7492374.63170.318.5774.9670.618.57
270254-7025469.98070.27
375785-7578575.49075.82
463957-6395763.70863.98
575974-7597475.67876.00
662604-6260462.36062.62
15min182792-8279282.47080.905.6383.2181.595.65
280796-8079680.48181.16
386069-8606985.73486.48
476937-7693776.63777.26
585741-8574185.40786.15
674955-7495574.66375.27
20min187791-8779187.44986.833.7088.6587.983.74
288124-8812487.78188.91
390436-9043690.08491.31
485064-8506484.73385.78
589792-8979289.44290.66
681831-8183181.51282.54
30min191535-9153591.17992.121.9892.8693.742.01
291009-9100990.65592.27
394504-9450494.13695.86
493522-9352293.15894.68
594171-9417193.80495.52
690113-9011389.76291.24
45min193236-9323692.87393.411.2195.0695.541.13
292200-9220091.84193.96
393206-9320692.84395.09
495389-9538995.01897.06
594068-9406893.70295.94
694534-9453494.16696.14
60min191327-9132790.97191.961.8393.6894.621.71
291867-9186791.50994.14
391199-9119990.84493.61
495657-9565795.28597.85
591586-9158691.22993.99
692277-9227791.91894.42
极限188595-8859588.25091.312.3491.4694.482.25
290348-9034889.99693.14
392143-9214391.78495.05
495003-9500394.63397.73
592321-9232191.96295.23
691609-9160991.25294.26
玛巴洛沙韦干混悬剂项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DQTL-4125-250109对照品来源自制对照品使用方法直接使用
对照品含量(%)99.77对照品水分(%)0对照品稀释倍数2500
标示量(mg)40供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.111000521000201000441000141001601000580.06
211.129970899700997040.01
单位质量响应值RSD%判断
9006.128966.190.32数据可信
供试品溶液-2025090921批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181432-8143281.37083.352.6581.3783.352.65
285540-8554085.47585.48
384640-8464084.57684.58
482089-8208982.02782.03
585894-8589485.82985.83
680867-8086780.80680.81
10min193739-9373993.66895.551.3094.1296.011.29
296182-9618296.10996.58
396075-9607596.00296.47
497353-9735397.27997.73
594891-9489194.81995.30
695469-9546995.39795.85
15min195422-9542295.35098.001.4396.3298.991.42
298518-9851898.44399.45
399361-9936199.286100.29
498954-9895498.87999.88
597950-9795097.87698.88
698226-9822698.15299.13
20min194738-9473894.66697.041.5496.1798.581.53
296853-9685396.78098.34
398668-9866898.593100.15
498355-9835598.28099.83
596172-9617296.09997.65
697886-9788697.81299.34
30min195810-9581095.73798.031.4997.77100.101.48
297924-9792497.85099.94
3100118-100118100.042102.14
499110-9911099.035101.13
597913-9791397.83999.92
697722-9772297.64899.72
45min187829-8782987.76295.614.0590.3298.233.97
296801-9680196.72899.36
397548-9754897.474100.13
496650-9665096.57799.22
597521-9752197.447100.07
697727-9772797.653100.26
60min195563-9556395.49196.711.3998.5499.861.38
296328-9632896.25599.43
397915-9791597.841101.04
498907-9890798.832102.01
596369-9636996.29699.46
695610-9561095.53898.69
极限193241-9324193.17094.641.3696.7598.331.35
296135-9613596.06299.77
394411-9441194.33998.08
494675-9467594.60398.33
596309-9630996.23699.94
693511-9351193.44097.12
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