叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389329093246927499304593192931040.24
210.389239292079922360.24
单位质量响应值RSD%判断
8969.568885.930.67数据可信
供试品溶液-21FA624批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111188-1118820.57321.639.7220.5721.639.71
211690-1169021.49621.50
310809-1080919.87619.88
411131-1113120.46820.47
511774-1177421.65021.65
613972-1397225.69225.69
10min122286-2228640.98039.502.8041.2139.742.77
221286-2128639.14139.38
321847-2184740.17240.39
421356-2135639.26939.50
520507-2050737.70837.95
621612-2161239.74040.03
15min126392-2639248.53048.421.0149.2149.101.03
226579-2657948.87449.55
325972-2597247.75748.42
426397-2639748.53949.20
526057-2605747.91448.57
626602-2660248.91649.64
20min129712-2971254.63453.352.5755.8654.572.55
229326-2932653.92555.14
327761-2776151.04752.24
429181-2918153.65854.86
528520-2852052.44353.63
629594-2959454.41855.69
30min133159-3315960.97357.558.2862.8059.358.04
232726-3272660.17761.99
332156-3215659.12960.89
426132-2613248.05249.85
531552-3155258.01859.79
632044-3204458.92360.80
45min135617-3561765.49364.181.4668.0066.631.42
234621-3462163.66166.15
334536-3453663.50565.93
435332-3533264.96967.30
534301-3430163.07365.49
635023-3502364.40066.93
60min137362-3736268.70167.571.3571.9470.741.29
236994-3699468.02571.22
336375-3637566.88670.01
437174-3717468.35671.41
536448-3644867.02170.14
636137-3613766.44969.69
90min139050-3905071.80574.473.4075.8078.393.20
241850-4185076.95480.90
339022-3902271.75475.62
442241-4224177.67381.49
540049-4004973.64277.51
640797-4079775.01879.00
极限142916-4291678.91476.145.0483.7180.884.68
239300-3930072.26577.07
343242-4324279.51384.18
442726-4272678.56583.24
541964-4196477.16481.85
638311-3831170.44675.26
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.389186492098919969195791892919610.11
210.389278892811928000.02
单位质量响应值RSD%判断
8859.448940.270.65数据可信
供试品溶液-21FA624批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min110854-1085420.02120.8910.5520.0220.8910.55
210648-1064819.64119.64
311328-1132820.89520.90
411480-1148021.17621.18
513540-1354024.97524.98
610092-1009218.61518.62
10min123297-2329742.97340.608.4743.2040.838.44
220526-2052637.86138.08
323743-2374343.79544.03
423686-2368643.69043.93
521513-2151339.68239.96
619285-1928535.57235.78
15min127256-2725650.27550.264.7350.9850.954.67
227668-2766851.03551.67
325874-2587447.72648.44
429473-2947354.36555.09
526138-2613848.21348.93
627087-2708749.96450.57
20min130348-3034855.97955.793.6057.2457.043.58
230022-3002255.37756.58
331611-3161158.30859.56
431338-3133857.80559.13
528865-2886553.24354.50
629296-2929654.03855.20
30min132621-3262160.17160.894.9962.0562.764.93
233448-3344861.69763.52
334930-3493064.43166.33
434698-3469864.00365.97
531229-3122957.60459.45
631148-3114857.45459.21
45min133397-3339761.60367.816.9264.1570.356.72
234126-3412662.94865.45
338041-3804170.16972.78
439378-3937872.63575.31
539107-3910772.13574.62
636537-3653767.39569.79
60min136787-3678767.85670.943.1371.0974.243.11
238064-3806470.21173.42
339555-3955572.96276.35
440074-4007473.91977.40
537785-3778569.69772.98
638503-3850371.02174.17
90min139202-3920272.31175.924.6976.3080.004.58
241556-4155676.65380.64
340629-4062974.94379.15
444772-4477282.58586.89
540149-4014974.05778.12
640638-4063874.95978.89
极限138685-3868571.35775.493.7976.1580.423.75
240344-4034474.41779.26
341271-4127176.12781.16
443339-4333979.94185.17
541561-4156176.66281.55
640368-4036874.46179.23
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