辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152703402690572692282688192688462692580.24
210.232689062683302686180.16
单位质量响应值RSD%判断
26527.8826257.870.73数据可信
供试品溶液-2025071721批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1204169-20416977.20575.511.6177.2075.511.60
2200666-20066675.88075.88
3200656-20065675.87775.88
4200277-20027775.73375.73
5197557-19755774.70574.70
6194767-19476773.65073.65
10min1230694-23069487.23586.831.6487.4787.061.64
2234916-23491688.83289.06
3227048-22704885.85686.08
4232440-23244087.89588.12
5227953-22795386.19986.42
6224742-22474284.98485.21
15min1242773-24277391.80390.761.6592.3091.251.64
2245370-24537092.78593.28
3236486-23648689.42589.91
4242238-24223891.60092.09
5237223-23722389.70490.19
6236012-23601289.24689.72
20min1246106-24610693.06392.201.5393.8392.961.54
2248578-24857893.99894.77
3240389-24038990.90191.65
4246504-24650493.21493.98
5241973-24197391.50092.25
6239429-23942990.53891.28
30min1247507-24750793.59392.761.5494.6493.791.54
2250392-25039294.68495.74
3241750-24175091.41692.44
4247789-24778993.69994.74
5243176-24317691.95592.98
6241186-24118691.20392.22
45min1248461-24846193.95493.161.4195.2894.471.41
2250339-25033994.66496.00
3242821-24282191.82193.12
4249446-24944694.32695.65
5244637-24463792.50893.81
6242485-24248591.69492.98
60min1247026-24702693.41192.901.3695.0294.491.36
2249883-24988394.49196.11
3242240-24224091.60193.18
4248493-24849393.96695.58
5244509-24450992.45994.04
6241840-24184091.45093.01
极限1265437-265437100.373100.780.87102.26102.660.88
2268390-268390101.490103.40
3263461-26346199.626101.48
4269603-269603101.948103.84
5267313-267313101.082102.94
6264911-264911100.174102.01
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152677682678432680062679252680332679150.05
210.232677192678652677920.04
单位质量响应值RSD%判断
26395.5726177.130.59数据可信
供试品溶液-2025071821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1202066-20206676.71975.791.9676.7275.791.96
2204856-20485677.77877.78
3198017-19801775.18175.18
4200850-20085076.25776.26
5198386-19838675.32175.32
6193553-19355373.48773.49
10min1229187-22918787.01686.282.2287.2586.512.22
2234744-23474489.12689.36
3227827-22782786.49986.72
4228366-22836686.70486.93
5223096-22309684.70384.93
6220300-22030083.64283.86
15min1242034-24203491.89391.302.1592.3891.792.14
2248880-24888094.49394.99
3240648-24064891.36791.85
4241101-24110191.53992.03
5235891-23589189.56190.04
6234298-23429888.95689.43
20min1246560-24656093.61293.411.8594.3894.171.85
2253457-25345796.23097.01
3246758-24675893.68794.45
4246885-24688593.73594.50
5241232-24123291.58992.34
6241213-24121391.58292.32
30min1247958-24795894.14394.701.8095.1995.741.80
2257515-25751597.77198.84
3250244-25024495.01096.05
4249924-24992494.88995.93
5244880-24488092.97494.00
6246028-24602893.41094.42
45min1248594-24859494.38495.041.6395.7196.361.62
2257613-25761397.80899.17
3251159-25115995.35896.68
4250324-25032495.04196.37
5245543-24554393.22694.53
6248716-24871694.43095.72
60min1248248-24824894.25394.721.8095.8796.341.80
2256977-25697797.56799.23
3251208-25120895.37696.99
4250262-25026295.01796.63
5244349-24434992.77294.35
6245898-24589893.36094.94
极限1270622-270622102.747102.961.20104.64104.851.19
2275082-275082104.441106.39
3271831-271831103.206105.10
4268519-268519101.949103.85
5266774-266774101.286103.15
6274280-274280104.136105.99
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152696082697072697132694902693612695760.06
210.232685032683152684090.05
单位质量响应值RSD%判断
26559.2126237.440.87数据可信
供试品溶液-2025071921批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1199238-19923875.32675.362.3875.3375.362.38
2204416-20441677.28377.28
3202680-20268076.62776.63
4190926-19092672.18372.18
5197927-19792774.83074.83
6200764-20076475.90375.90
10min1233076-23307688.11987.731.1288.3487.961.12
2230238-23023887.04687.28
3230913-23091387.30187.53
4228489-22848986.38486.60
5234567-23456788.68288.91
6235047-23504788.86489.09
15min1242884-24288491.82791.260.8592.3291.750.85
2240420-24042090.89591.39
3238581-23858190.20090.69
4240161-24016190.79791.27
5242114-24211491.53692.03
6244166-24416692.31192.81
20min1246240-24624093.09692.831.3593.8693.591.34
2243808-24380892.17692.94
3240628-24062890.97491.74
4244358-24435892.38493.13
5248708-24870894.02994.79
6249482-24948294.32195.09
30min1248739-24873994.04093.401.3795.0994.451.36
2244704-24470492.51593.56
3243671-24367192.12493.16
4245361-24536192.76393.79
5246941-24694193.36194.41
6252911-25291195.61896.67
45min1247644-24764493.62693.160.9694.9594.480.95
2244916-24491692.59593.91
3243008-24300891.87493.19
4245311-24531192.74494.05
5248677-24867794.01795.34
6248831-24883194.07595.42
60min1248115-24811593.80493.110.9295.4194.720.92
2243553-24355392.08093.68
3243706-24370692.13893.72
4246050-24605093.02494.61
5247399-24739993.53495.14
6248915-24891594.10795.73
极限1262508-26250899.24699.820.51101.14101.700.50
2265816-265816100.497102.37
3262562-26256299.266101.13
4264344-26434499.940101.80
5265124-265124100.235102.12
6263861-26386199.757101.66
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