辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152724002726162730472726862727472726990.09
210.232691732697912694820.17
单位质量响应值RSD%判断
26866.9026342.331.40数据可信
供试品溶液-2025071721批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1202611-20261176.01176.251.7576.0176.261.75
2207446-20744677.82577.83
3202204-20220475.85975.86
4203182-20318276.22676.23
5206582-20658277.50177.50
6197513-19751374.09974.10
10min1229188-22918885.98287.421.4786.2187.651.47
2234912-23491288.12988.36
3235587-23558788.38388.61
4231003-23100386.66386.89
5237482-23748289.09489.33
6229964-22996486.27386.50
15min1238438-23843889.45291.051.4589.9491.541.45
2243955-24395591.52292.02
3245669-24566992.16592.66
4239311-23931189.78090.27
5247200-24720092.73993.24
6241650-24165090.65791.14
20min1240589-24058990.25992.291.5791.0193.061.57
2247465-24746592.83993.61
3249857-24985793.73694.51
4242691-24269191.04891.81
5250062-25006293.81394.59
6245413-24541392.06992.82
30min1242532-24253290.98892.941.6992.0193.981.69
2248374-24837493.18094.23
3252550-25255094.74795.80
4243004-24300491.16592.20
5251406-25140694.31795.38
6248570-24857093.25394.28
45min1244001-24400191.53993.281.3392.8494.601.33
2249072-24907293.44294.77
3250789-25078994.08695.42
4245529-24552992.11393.42
5252816-25281694.84696.19
6249677-24967793.66994.98
60min1243994-24399491.53793.101.3293.1194.701.31
2248643-24864393.28194.89
3252116-25211694.58496.20
4244474-24447491.71793.30
5250115-25011593.83395.46
6249648-24964893.65895.25
极限1274821-274821103.102101.551.18104.95103.431.17
2269389-269389101.064102.95
3271673-271673101.921103.82
4266820-266820100.100101.96
5273556-273556102.627104.54
6267890-267890100.501102.37
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152689232689422700012693382691002692610.17
210.232688742685282687010.10
单位质量响应值RSD%判断
26528.1826265.980.71数据可信
供试品溶液-2025071821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1201049-20104976.01376.432.8776.0176.432.87
2206032-20603277.89777.90
3202240-20224076.46376.46
4195513-19551373.92073.92
5211123-21112379.82279.82
6196949-19694974.46374.46
10min1218248-21824882.51686.022.5782.7486.252.57
2233152-23315288.15088.38
3228497-22849786.39086.62
4224697-22469784.95485.18
5234088-23408888.50488.74
6226473-22647385.62585.85
15min1229861-22986186.90691.062.5187.3891.552.51
2246223-24622393.09293.59
3240081-24008190.77091.26
4240256-24025690.83691.31
5246232-24623293.09693.60
6242457-24245791.66892.15
20min1234878-23487888.80392.592.2189.5493.352.21
2250210-25021094.60095.38
3244371-24437192.39293.15
4244482-24448292.43493.18
5248133-24813393.81494.60
6247303-24730393.50194.26
30min1239032-23903290.37493.761.9791.3894.801.97
2252789-25278995.57596.64
3246712-24671293.27794.32
4248379-24837993.90794.93
5251356-25135695.03396.10
6249667-24966794.39495.43
45min1240811-24081191.04694.101.7592.3295.421.75
2253712-25371295.92497.27
3248394-24839493.91395.23
4249518-24951894.33895.65
5250769-25076994.81196.16
6250202-25020294.59795.92
60min1241441-24144191.28494.091.6992.8395.701.69
2253645-25364595.89897.53
3248144-24814493.81995.42
4248121-24812193.81095.40
5251033-25103394.91196.55
6250858-25085894.84596.45
极限1272041-272041102.854102.901.13104.67104.791.11
2274764-274764103.883105.81
3268284-268284101.433103.31
4276010-276010104.354106.23
5272851-272851103.160105.08
6269092-269092101.739103.63
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152698802696992701252698272701702699400.08
210.232708552697562703060.29
单位质量响应值RSD%判断
26595.0726422.870.46数据可信
供试品溶液-2025071921批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1204865-20486577.12875.973.0377.1375.973.03
2210047-21004779.07979.08
3205315-20531577.29777.30
4194408-19440873.19173.19
5200647-20064775.54075.54
6195440-19544073.57973.58
10min1233480-23348087.90187.102.5688.1387.322.57
2238817-23881789.91090.15
3233796-23379688.02088.25
4227962-22796285.82386.04
5232475-23247587.52287.75
6221536-22153683.40483.62
15min1244822-24482292.17190.932.8792.6791.422.87
2250003-25000394.12194.63
3243907-24390791.82692.32
4238471-23847189.78090.26
5242237-24223791.19791.69
6229657-22965786.46186.93
20min1247942-24794293.34592.262.2594.1293.022.26
2253422-25342295.40896.20
3245307-24530792.35393.12
4242450-24245091.27892.02
5244333-24433391.98792.75
6236935-23693589.20189.93
30min1248642-24864293.60992.672.8194.6693.712.81
2255339-25533996.13097.21
3247266-24726693.09194.14
4245014-24501492.24393.26
5246608-24660892.84393.88
6234077-23407788.12589.12
45min1249875-24987594.07392.852.8195.4194.172.80
2256062-25606296.40297.77
3245626-24562692.47393.80
4247029-24702993.00294.30
5246259-24625992.71294.03
6234897-23489788.43489.70
60min1249375-24937593.88592.652.8095.5094.242.80
2255391-25539196.15097.80
3247295-24729593.10294.71
4245387-24538792.38393.96
5244647-24464792.10593.70
6234441-23444188.26289.79
极限1266279-266279100.249100.541.81102.15102.421.79
2275929-275929103.882105.82
3264032-26403299.403101.29
4266737-266737100.421102.27
5261858-26185898.584100.46
6267522-267522100.717102.51
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