辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882658252657522655972660172659372658260.07
29.922674582673212673900.04
单位质量响应值RSD%判断
26905.4726954.640.13数据可信
供试品溶液-2025071821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1193556-19355671.73072.084.1471.7372.084.14
2188649-18864969.91169.91
3198671-19867173.62573.63
4189504-18950470.22870.23
5187946-18794669.65169.65
6208756-20875677.36377.36
10min1215209-21520979.75483.543.2079.9783.763.19
2227270-22727084.22484.43
3218272-21827280.88981.11
4231145-23114585.66085.87
5227288-22728884.23184.44
6233403-23340386.49786.73
15min1226329-22632983.87585.902.1884.3386.362.18
2229107-22910784.90585.37
3229952-22995285.21885.68
4230696-23069685.49485.96
5233802-23380286.64587.11
6240785-24078589.23389.72
20min1229709-22970985.12887.293.0685.8388.023.06
2226634-22663483.98884.71
3233934-23393486.69487.41
4240868-24086889.26389.99
5235863-23586387.40888.13
6246276-24627691.26792.03
30min1245315-24531590.91189.771.8491.8790.751.83
2235931-23593187.43488.40
3244810-24481090.72491.70
4242149-24214989.73890.73
5237973-23797388.19089.17
6247158-24715891.59492.63
45min1240643-24064389.18090.621.6090.4191.881.60
2239492-23949288.75389.98
3243898-24389890.38691.64
4248196-24819691.97993.24
5246054-24605491.18592.43
6248908-24890892.24393.55
60min1237129-23712987.87890.662.0289.3892.192.01
2246366-24636691.30192.80
3245663-24566391.04092.56
4247361-24736191.67093.21
5240572-24057289.15490.68
6250703-25070392.90894.49
极限1260577-26057796.56798.432.1898.33100.232.18
2260044-26004496.37098.14
3262849-26284997.40999.20
4271647-271647100.670102.48
5264830-26483098.14399.93
6273753-273753101.450103.31
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882665902667512667242668382669452667700.05
29.922686842683752685300.09
单位质量响应值RSD%判断
27001.0127069.560.18数据可信
供试品溶液-2025071821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1199533-19953373.65769.443.4573.6669.443.45
2186153-18615368.71868.72
3186952-18695269.01369.01
4187101-18710169.06869.07
5189272-18927269.86969.87
6179654-17965466.31966.32
10min1223791-22379182.61283.165.5682.8383.365.55
2229764-22976484.81785.02
3222942-22294282.29982.51
4217812-21781280.40580.61
5247024-24702491.18891.40
6210259-21025977.61777.82
15min1230271-23027185.00484.302.0385.4784.762.03
2234473-23447386.55587.02
3222530-22253082.14682.60
4231602-23160285.49585.94
5227516-22751683.98784.47
6223816-22381682.62183.05
20min1234555-23455586.58586.642.4087.3187.352.39
2238826-23882688.16288.88
3225136-22513683.10883.81
4235251-23525186.84287.55
5241470-24147089.13889.87
6233024-23302486.02086.70
30min1240289-24028988.70289.271.1689.6990.241.15
2245090-24509090.47491.46
3238322-23832287.97688.93
4245047-24504790.45991.42
5240026-24002688.60589.61
6242247-24224789.42590.36
45min1235700-23570087.00888.521.7788.2689.761.76
2247181-24718191.24692.50
3237565-23756587.69788.91
4241147-24114789.01990.26
5240748-24074888.87290.14
6236483-23648387.29788.50
60min1241092-24109288.99989.872.5390.5191.382.49
2247438-24743891.34192.87
3233929-23392986.35487.83
4243786-24378689.99391.50
5242384-24238489.47691.01
6252138-25213893.07694.54
极限1263772-26377297.37198.261.3099.15100.041.29
2272526-272526100.602102.41
3266049-26604998.21199.95
4265976-26597698.18499.96
5266176-26617698.258100.06
6262596-26259696.93798.68
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882629302629492629932630472631382630110.04
29.922653772650482652120.09
单位质量响应值RSD%判断
26620.5526735.080.31数据可信
供试品溶液-2025071821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1186073-18607369.60967.626.8169.6167.626.81
2184324-18432468.95568.95
3197641-19764173.93773.94
4161054-16105460.25060.25
5181130-18113067.76067.76
6174230-17423065.17965.18
10min1219186-21918681.99680.254.2982.2180.464.29
2211814-21181479.23979.45
3216508-21650880.99581.22
4197404-19740473.84874.03
5223253-22325383.51883.72
6218940-21894081.90482.10
15min1226254-22625484.64183.241.8385.1083.691.83
2222459-22245983.22183.67
3221551-22155182.88183.35
4219376-21937682.06882.47
5228086-22808685.32685.78
6217373-21737381.31881.76
20min1224612-22461284.02685.293.3784.7485.993.37
2230817-23081786.34887.04
3234598-23459887.76288.48
4214796-21479680.35481.00
5235526-23552688.10988.82
6227655-22765585.16585.85
30min1232297-23229786.90186.121.9387.8687.071.95
2232166-23216686.85287.81
3235388-23538888.05889.03
4223002-22300283.42484.31
5231405-23140586.56887.54
6227021-22702184.92885.87
45min1247757-24775792.68591.051.5993.9192.251.55
2239937-23993789.75990.97
3237992-23799289.03290.27
4246031-24603192.03993.18
5242613-24261390.76091.99
6245938-24593892.00493.20
60min1247755-24775592.68490.391.4494.1891.871.41
2238639-23863989.27490.76
3238454-23845489.20590.71
4242719-24271990.80092.22
5241986-24198690.52692.03
6240233-24023389.87091.34
极限1258173-25817396.58195.531.7598.3697.281.73
2261961-26196197.99899.75
3251826-25182694.20795.98
4249458-24945893.32195.01
5255473-25547395.57197.35
6255257-25525795.49097.23
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