诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 9.553739199373874537342703736450373400937365350.07
2 9.583767433375576937616010.22
单位质量响应值RSD%判断
391260.21392651.460.26数据可信
供试品溶液-25032批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1197948-1979484.5274.9129.624.534.9229.60
2237485-2374855.4315.43
395645-956452.1872.19
4273083-2730836.2456.25
5254875-2548755.8295.83
6229821-2298215.2565.26
10min1884947-88494720.23921.8714.7620.2521.8814.76
21068936-106893624.44724.46
3706064-70606416.14816.15
41055212-105521224.13324.14
5971549-97154922.21922.23
61051722-105172224.05324.06
15min11563295-156329535.75338.3411.6135.7938.3911.61
21884969-188496943.10943.16
31358822-135882231.07631.11
41783522-178352240.78940.84
51650968-165096837.75837.80
61817901-181790141.57541.62
20min12197577-219757750.25953.389.6750.3653.499.68
22610564-261056459.70459.83
31983714-198371445.36845.45
42426650-242665055.49755.62
52289771-228977152.36752.48
62495169-249516957.06557.18
30min13219428-321942873.62876.046.4573.8176.246.46
23623338-362333882.86683.09
32992880-299288068.44768.61
43364740-336474076.95277.16
53294840-329484075.35375.55
63453645-345364578.98579.20
45min14046871-404687192.55293.263.3492.8693.583.36
24238636-423863696.93897.30
33840984-384098487.84388.12
44060501-406050192.86493.20
54111608-411160894.03294.36
64168150-416815095.32695.67
60min14362673-436267399.77499.262.09100.2499.742.12
24396069-4396069100.538101.06
34166317-416631795.28495.70
44330690-433069099.04399.54
54363253-436325399.788100.27
64421533-4421533101.120101.62
极限14491065-4491065102.711101.171.38103.34101.821.40
24431783-4431783101.355102.04
34308695-430869598.54099.12
44448819-4448819101.744102.40
54433968-4433968101.405102.05
64428570-4428570101.281101.95
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