熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.335350453207537405348953132534140.47
211.345395053486537180.62
单位质量响应值RSD%判断
4714.394737.040.34数据可信
供试品溶液-J223批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min110502-1050219.92119.5514.6819.9219.5514.68
210896-1089620.66820.67
37328-732813.90013.90
410560-1056020.03120.03
511616-1161622.03422.03
610937-1093720.74620.75
10min111753-1175322.29420.8715.6722.3320.9015.67
211073-1107321.00421.04
37659-765914.52814.55
411210-1121021.26421.30
512595-1259523.89123.93
611726-1172622.24322.28
15min112007-1200722.77621.1716.1322.8521.2416.11
211036-1103620.93421.00
37712-771214.62914.68
411347-1134721.52421.59
512820-1282024.31824.39
612040-1204022.83822.91
20min112038-1203822.83421.3316.4222.9421.4316.42
211163-1116321.17521.28
37765-776514.72914.80
411202-1120221.24921.35
513057-1305724.76724.88
612253-1225323.24223.35
30min112441-1244123.59921.6516.5323.7521.7916.53
211305-1130521.44421.58
37859-785914.90715.00
411342-1134221.51421.65
513223-1322325.08225.24
612309-1230923.34923.50
45min112577-1257723.85721.9617.2624.0422.1317.26
211458-1145821.73421.91
37799-779914.79414.91
411480-1148021.77621.95
513379-1337925.37825.58
612759-1275924.20224.39
60min112781-1278124.24422.0817.5324.4722.3017.51
211680-1168022.15522.37
37781-778114.76014.91
411481-1148121.77821.99
513585-1358525.76926.01
612544-1254423.79424.02
极限112846-1284624.36722.1918.1624.6322.4318.13
211837-1183722.45322.70
37673-767314.55514.73
411405-1140521.63421.88
513634-1363425.86226.15
612781-1278124.24424.51
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.335229952162525365245651828522560.54
211.345277153016528940.33
单位质量响应值RSD%判断
4612.184664.370.80数据可信
供试品溶液-J223批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11153-11532.2282.307.612.232.307.60
21065-10652.0582.06
31140-11402.2032.20
41256-12562.4272.43
51196-11962.3112.31
61320-13202.5512.55
10min12293-22934.4323.759.404.443.769.41
21928-19283.7263.73
31760-17603.4023.41
41887-18873.6473.65
51862-18623.5993.60
61922-19223.7153.72
15min12126-21264.1094.102.474.124.112.49
22169-21694.1924.20
32147-21474.1494.16
42024-20243.9123.92
52152-21524.1594.17
62103-21034.0644.07
20min12215-22154.2814.343.844.304.363.79
22306-23064.4574.47
32138-21384.1324.15
42207-22074.2654.28
52223-22234.2964.31
62383-23834.6064.62
30min12226-22264.3024.533.324.334.553.28
22302-23024.4494.47
32461-24614.7564.78
42349-23494.5404.56
52370-23704.5804.60
62359-23594.5594.58
45min12552-25524.9325.0714.774.965.1014.68
22299-22994.4434.47
32517-25174.8654.90
43395-33956.5616.59
52527-25274.8844.92
62463-24634.7604.79
60min12556-25564.9404.753.014.984.793.00
22369-23694.5794.62
32423-24234.6834.72
42541-25414.9114.95
52429-24294.6944.73
62429-24294.6944.73
极限12648-26485.1184.833.795.174.883.78
22491-24914.8144.86
32372-23724.5844.63
42537-25374.9034.95
52432-24324.7004.75
62516-25164.8634.91
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.335229852777523485224651752522840.70
211.345283852581527100.35
单位质量响应值RSD%判断
4614.654648.150.52数据可信
供试品溶液-J223批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13664-36647.0927.478.657.097.478.65
23691-36917.1447.14
33662-36627.0887.09
44496-44968.7028.70
53970-39707.6847.68
63674-36747.1117.11
10min14309-43098.3408.082.078.358.092.07
24120-41207.9747.99
34176-41768.0838.09
44240-42408.2078.22
54082-40827.9017.91
64119-41197.9727.98
15min14446-44468.6058.292.298.638.322.26
24254-42548.2348.26
34334-43348.3888.41
44159-41598.0508.08
54281-42818.2868.31
64233-42338.1938.22
20min14435-44358.5848.431.168.628.461.13
24338-43388.3968.44
34371-43718.4608.50
44313-43138.3488.39
54294-42948.3118.35
64367-43678.4528.49
30min14466-44668.6448.491.948.708.541.93
24307-43078.3368.39
34444-44448.6018.65
44330-43308.3818.44
54477-44778.6658.72
64294-42948.3118.36
45min14471-44718.6548.522.588.728.592.57
24455-44558.6238.69
34360-43608.4398.51
44411-44118.5388.61
54525-45258.7588.83
64203-42038.1358.20
60min14423-44238.5618.482.588.648.562.54
24382-43828.4818.56
34454-44548.6218.70
44331-43318.3838.47
54502-45028.7148.80
64183-41838.0968.18
极限14372-43728.4628.452.998.568.542.99
24380-43808.4788.57
34434-44348.5828.68
44368-43688.4548.55
54510-45108.7298.83
64122-41227.9788.07
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.335348353883539605385253934538220.37
211.345416153789539750.49
单位质量响应值RSD%判断
4750.404759.700.14数据可信
供试品溶液-J223批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min145387-4538785.56286.131.1885.5686.141.18
245766-4576686.27686.28
344790-4479084.43684.44
445799-4579986.33886.34
546190-4619087.07587.08
646209-4620987.11187.11
10min149804-4980493.88893.360.9194.0393.500.91
249415-4941593.15593.30
348658-4865891.72891.87
449761-4976193.80793.95
549739-4973993.76693.91
649766-4976693.81793.96
15min150485-5048595.17295.011.8495.4795.311.84
251444-5144496.98097.28
348727-4872791.85892.15
450371-5037194.95795.26
551028-5102896.19696.50
650327-5032794.87495.18
20min150536-5053695.26895.280.9795.7395.740.97
250511-5051195.22195.68
349794-4979493.86994.32
450368-5036894.95295.41
551275-5127596.66197.12
650774-5077495.71796.18
30min150747-5074795.66695.600.9896.2896.210.99
250586-5058695.36395.98
349869-4986994.01194.61
451040-5104096.21896.84
551340-5134096.78497.41
650681-5068195.54296.16
45min150987-5098796.11895.651.0296.8996.431.02
250674-5067495.52896.31
349848-4984893.97194.73
450755-5075595.68196.46
551417-5141796.92997.71
650753-5075395.67796.46
60min150858-5085895.87596.732.2996.8197.662.26
250759-5075995.68996.63
353646-53646101.131102.05
450847-5084795.85596.79
551278-5127896.66797.61
650479-5047995.16196.10
极限151664-5166497.39597.350.8398.4998.450.82
251834-5183497.71598.81
350968-5096896.08397.17
451632-5163297.33498.43
552265-5226598.52899.63
651492-5149297.07098.17
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