布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.302727490272657527264732725839272658427265920.03
211.252728049272582327269360.06
单位质量响应值RSD%判断
241291.33242394.310.33数据可信
供试品溶液-2025082451批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12705772-2705772100.59395.412.98100.5995.412.97
22591703-259170396.35296.35
32539715-253971594.42094.42
42556090-255609095.02895.03
52507302-250730293.21593.21
62497919-249791992.86692.87
10min12698609-2698609100.32795.972.88101.4497.032.88
22629271-262927197.74998.82
32549694-254969494.79195.84
42591371-259137196.34097.40
52504494-250449493.11094.15
62514517-251451793.48394.51
15min12657854-265785498.81295.462.33101.0497.582.34
22612436-261243697.12399.28
32535650-253565094.26896.37
42572228-257222895.62897.75
52493654-249365492.70794.78
62534418-253441894.22396.29
20min12639436-263943698.12794.842.25101.4698.022.26
22596440-259644096.52899.76
32517888-251788893.60896.76
42552912-255291294.91098.10
52495686-249568692.78395.88
62503081-250308193.05896.18
30min12630449-263044997.79394.302.36102.2198.542.37
22587957-258795796.213100.52
32506346-250634693.17997.37
42523299-252329993.80998.05
52478566-247856692.14696.28
62492291-249229192.65696.81
极限12610781-261078197.06293.232.66102.5798.522.65
22561005-256100595.211100.59
32489532-248953292.55497.78
42496989-249698992.83198.12
52448506-244850691.02996.18
62438945-243894590.67395.85
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.302725477272518527257942725622272592127256000.02
211.252722646272019327214200.07
单位质量响应值RSD%判断
241203.54241904.000.21数据可信
供试品溶液-2025082451批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12363252-236325287.96493.273.8487.9693.273.84
22550255-255025594.92594.92
32407144-240714489.59889.60
42558295-255829595.22495.22
52598811-259881196.73296.73
62557496-255749695.19495.19
10min12401670-240167089.39493.543.2190.3794.573.21
22569542-256954295.64296.70
32421792-242179290.14391.14
42537753-253775394.45995.52
52589811-258981196.39797.47
62557276-255727695.18696.24
15min12387550-238755088.86893.103.2190.8495.183.22
22541451-254145194.59796.71
32410980-241098089.74191.74
42552024-255202494.99097.10
52573342-257334295.78497.93
62542646-254264694.64196.76
20min12374631-237463188.38892.653.4091.3595.763.40
22542905-254290594.65197.82
32387051-238705188.85091.84
42538825-253882594.49997.66
52559792-255979295.28098.49
62531312-253131294.21997.39
30min12358107-235810787.77391.723.4091.7195.863.40
22500797-250079793.08497.30
32357696-235769687.75791.74
42524664-252466493.97298.19
52542303-254230394.62998.90
62501278-250127893.10297.32
极限12344393-234439387.26291.343.2892.1896.503.28
22487991-248799192.60797.86
32359824-235982487.83692.79
42507234-250723493.32398.58
52530329-253032994.18399.50
62493553-249355392.81498.06
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.302723055272473427260172727981272472927253030.07
211.252719871272151127206910.05
单位质量响应值RSD%判断
241177.26241839.200.20数据可信
供试品溶液-2025082451批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12446954-244695491.09792.032.1091.1092.032.10
22503420-250342093.19993.20
32486872-248687292.58392.58
42377924-237792488.52788.53
52514315-251431593.60493.60
62502704-250270493.17293.17
10min12427671-242767190.37990.872.2591.3991.892.25
22477989-247798992.25293.29
32428763-242876390.41991.45
42342746-234274687.21788.20
52490033-249003392.70093.74
62477239-247723992.22493.26
15min12352102-235210287.56689.312.3189.5891.342.31
22414087-241408789.87391.93
32409542-240954289.70491.74
42315114-231511486.18888.14
52460850-246085091.61493.68
62442732-244273290.94093.00
20min12398173-239817389.28189.102.3992.2792.132.38
22441081-244108190.87893.94
32383502-238350288.73491.76
42285681-228568185.09388.00
52434951-243495190.65093.74
62416958-241695889.98093.05
30min12330867-233086786.77587.282.1990.7691.302.16
22389815-238981588.97093.04
32353368-235336887.61391.63
42266257-226625784.37088.23
52319053-231905386.33590.43
62407826-240782689.64093.71
极限12321700-232170086.43487.121.9891.3892.101.98
22364948-236494888.04493.10
32330771-233077186.77191.76
42261249-226124984.18388.98
52388000-238800088.90293.96
62373526-237352688.36393.43
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