他达拉非片项目信息
介质体积(ml)1000取样体积(ml) 0补液体积(ml) 0
对照品批号D533-190826对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.93对照品水分(%)0对照品稀释倍数2500
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.345154075156685151715155835159925155640.06
212.375158435153445155940.07
单位质量响应值RSD%判断
41779.9041681.000.17数据可信
供试品溶液-2025091821批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121737-217374.1644.9717.004.164.9717.01
228006-280065.3655.37
327082-270825.1885.19
422195-221954.2524.25
533213-332136.3636.36
623321-233214.4684.47
10min148655-486559.3219.438.349.329.438.36
249249-492499.4359.43
350099-500999.5989.60
443867-438678.4048.40
556317-5631710.78910.79
647194-471949.0419.04
15min161667-6166711.81411.935.2611.8111.935.26
263103-6310312.08912.09
362075-6207511.89211.89
457836-5783611.08011.08
567858-6785813.00013.00
661031-6103111.69211.69
20min169575-6957513.32913.523.4513.3313.523.46
270694-7069413.54313.54
370313-7031313.47013.47
467713-6771312.97212.97
575064-7506414.38014.38
670116-7011613.43213.43
30min178391-7839115.01815.322.0115.0215.322.02
279952-7995215.31715.32
379712-7971215.27115.27
478726-7872615.08215.08
582924-8292415.88615.89
680140-8014015.35315.35
45min184043-8404316.10016.561.7516.1016.561.75
287190-8719016.70316.70
385816-8581616.44016.44
486243-8624316.52216.52
588533-8853316.96016.96
686965-8696516.66016.66
极限190103-9010317.26117.681.4317.2617.681.43
292306-9230617.68317.68
392066-9206617.63717.64
492130-9213017.65017.65
594116-9411618.03018.03
692979-9297917.81217.81
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