熊取样胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.945210452252521735207951977521170.20
214.035299153048530200.08
单位质量响应值RSD%判断
3738.673779.040.76数据可信
供试品溶液-25102801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142552-4255281.18479.393.1981.1879.393.19
242902-4290281.85181.85
341977-4197780.08780.09
439891-3989176.10776.11
542347-4234780.79380.79
640000-4000076.31576.31
10min148811-4881193.12592.820.8093.2692.950.80
249122-4912293.71893.85
348707-4870792.92793.06
448015-4801591.60691.73
548837-4883793.17593.31
648408-4840892.35692.48
15min150502-5050296.35196.020.3296.6496.310.32
250265-5026595.89996.19
350180-5018095.73796.03
450198-5019895.77196.05
550556-5055696.45496.74
650280-5028095.92896.21
20min150577-5057796.49496.570.5296.9597.020.52
250311-5031195.98796.44
350493-5049396.33496.78
450752-5075296.82897.27
551067-5106797.42997.88
650506-5050696.35996.80
30min150588-5058896.51596.680.4897.1397.290.47
250342-5034296.04696.66
350599-5059996.53697.14
450812-5081296.94397.54
551050-5105097.39798.01
650665-5066596.66297.26
45min150708-5070896.74496.630.5597.5297.400.55
250124-5012495.63096.40
350638-5063896.61197.38
450840-5084096.99697.76
550901-5090197.11297.89
650664-5066496.66097.42
60min150556-5055696.45496.480.6097.3997.410.59
250031-5003195.45396.38
350579-5057996.49897.43
450749-5074996.82297.75
550920-5092097.14998.09
650587-5058796.51397.44
极限150504-5050496.35596.350.6197.4597.440.61
249913-4991395.22896.32
350504-5050496.35597.45
450709-5070996.74697.83
550772-5077296.86697.97
650596-5059696.53197.62
熊取样胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数250
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.945307353006530385290552926529900.14
214.035309553033530640.09
单位质量响应值RSD%判断
3801.293782.180.36数据可信
供试品溶液-25102802批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min138226-3822672.29678.136.6172.3078.136.61
238183-3818372.21572.21
340501-4050176.59976.60
444320-4432083.82283.82
543594-4359482.44982.45
643036-4303681.39381.39
10min146759-4675988.43491.752.8388.5591.882.83
247301-4730189.46089.58
348049-4804990.87491.00
450296-5029695.12495.26
549543-4954393.70093.84
649112-4911292.88593.02
15min149117-4911792.89494.981.5393.1695.261.54
250016-5001694.59494.86
349839-4983994.26094.54
451404-5140497.22097.52
550538-5053895.58295.88
650395-5039595.31195.60
20min149815-4981594.21496.351.7294.6496.791.72
250915-5091596.29596.72
350182-5018294.90895.34
451604-5160497.59898.06
550959-5095996.37896.83
652175-5217598.67899.13
30min150124-5012494.79996.241.1295.3896.841.13
251292-5129297.00897.60
350314-5031495.15895.75
451596-5159697.58398.21
551060-5106096.56997.18
650933-5093396.32996.94
45min150311-5031195.15296.341.0495.8997.101.04
251316-5131697.05397.80
350293-5029395.11895.87
451542-5154297.48198.27
550975-5097596.40897.18
651182-5118296.80097.57
60min150226-5022694.99296.401.1195.8997.321.12
251393-5139397.19998.11
350351-5035195.22896.14
451633-5163397.65398.60
551071-5107196.59097.52
651153-5115396.74597.68
极限150216-5021694.97396.020.9996.0397.100.99
250916-5091696.29797.37
350197-5019794.93796.01
451449-5144997.30598.42
550719-5071995.92497.02
651116-5111696.67597.77
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