非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号C5654-24-004M2对照品来源中检院对照品使用方法直接使用
对照品含量(%) 98.3对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.103069783068053063333064753068493066880.09
211.173058903056613057760.06
单位质量响应值RSD%判断
27629.5527374.750.66数据可信
供试品溶液-25103101-1批-恩格列净-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min157191-5719118.39817.4915.1618.4017.5015.16
238102-3810212.25712.26
353773-5377317.29817.30
459612-5961219.17719.18
558835-5883518.92718.93
658744-5874418.89718.90
10min166171-6617121.28720.156.2421.3220.186.26
255056-5505617.71117.73
363799-6379920.52420.55
463094-6309420.29720.33
564808-6480820.84820.88
662946-6294620.24920.28
15min166691-6669121.45420.514.4621.5220.584.48
258533-5853318.83018.88
364053-6405320.60520.67
465848-6584821.18321.25
563539-6353920.44020.51
663898-6389820.55520.62
20min166689-6668921.45320.821.6221.5620.911.63
264757-6475720.83220.91
363605-6360520.46120.56
464292-6429220.68220.78
564354-6435420.70220.80
664557-6455720.76720.87
30min164404-6440420.71820.660.7120.8620.790.68
264792-6479220.84320.96
363586-6358620.45520.59
464250-6425020.66920.80
564452-6445220.73420.87
663761-6376120.51120.65
45min163508-6350820.43020.321.2820.6020.481.27
264046-6404620.60320.75
362135-6213519.98820.15
462308-6230820.04420.21
563001-6300120.26720.44
663905-6390520.55820.73
60min163736-6373620.50320.191.0520.7120.391.05
262891-6289120.23120.42
362220-6222020.01620.21
461919-6191919.91920.12
562595-6259520.13620.34
663145-6314520.31320.52
极限162826-6282620.21120.070.6720.4520.300.66
262638-6263820.15020.37
362134-6213419.98820.22
462482-6248220.10020.34
561685-6168519.84320.08
662560-6256020.12520.36
非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号250201对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
122.107762977773407772057768827785077772460.11
222.147761117750707755900.10
单位质量响应值RSD%判断
35169.5035031.170.28数据可信
供试品溶液-25103101-1批-非奈利酮-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min131547-315478.0898.5122.068.098.5122.05
238198-381989.7949.79
326526-265266.8026.80
444268-4426811.35111.35
533882-338828.6888.69
624685-246856.3296.33
10min157394-5739414.71614.9814.9614.7314.9914.98
264800-6480016.61516.63
355690-5569014.27914.29
466299-6629917.00017.02
563541-6354116.29216.31
642795-4279510.97310.98
15min176232-7623219.54719.0613.6319.5819.0913.62
277404-7740419.84719.89
373851-7385118.93618.97
482538-8253821.16321.21
581172-8117220.81320.85
654703-5470314.02614.06
20min189875-8987523.04522.6513.7623.1222.7213.76
2100571-10057125.78725.86
386615-8661522.20922.28
489942-8994223.06223.14
597181-9718124.91824.99
665915-6591516.90116.95
30min1106907-10690727.41226.9014.2427.5227.0114.24
2120373-12037330.86530.98
3105930-10593027.16127.27
4102175-10217526.19926.32
5116316-11631629.82429.94
677820-7782019.95420.03
45min1123436-12343631.65030.7311.7031.8030.8811.70
2135585-13558534.76534.94
3118862-11886230.47730.63
4118104-11810430.28330.45
5128559-12855932.96433.13
694512-9451224.23424.35
60min1133134-13313434.13732.779.1234.3432.979.14
2139083-13908335.66235.89
3128249-12824932.88433.08
4123959-12395931.78432.00
5135723-13572334.80135.02
6106694-10669427.35727.51
极限1144377-14437737.02035.376.0637.2835.626.09
2144955-14495537.16837.46
3134859-13485934.57934.83
4135655-13565534.78335.05
5144102-14410236.94937.23
6123613-12361331.69531.90
非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号C5654-24-004M2对照品来源中检院对照品使用方法直接使用
对照品含量(%) 98.3对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.103084443084703082223083513074773081930.14
211.173075293080393077840.12
单位质量响应值RSD%判断
27765.1427554.520.54数据可信
供试品溶液-25103101-2-1批-恩格列净-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min149133-4913315.71514.4021.7715.7214.4021.77
250652-5065216.20116.20
346660-4666014.92414.92
439832-3983212.74012.74
555720-5572017.82217.82
628077-280778.9818.98
10min154930-5493017.57019.036.9317.6019.066.94
262243-6224319.90919.94
361714-6171419.74019.76
461276-6127619.59919.62
563207-6320720.21720.25
653601-5360117.14517.16
15min155097-5509717.62319.875.6417.6819.925.62
262521-6252119.99820.06
363640-6364020.35620.41
463044-6304420.16520.22
564055-6405520.48820.55
664340-6434020.57920.62
20min155276-5527617.68019.915.7617.7720.005.72
262663-6266320.04320.14
363251-6325120.23120.32
462839-6283920.09920.19
563951-6395120.45520.55
665577-6557720.97521.05
30min153952-5395217.25720.197.4917.3720.317.46
263876-6387620.43120.56
364014-6401420.47520.60
464546-6454620.64520.77
564400-6440020.59920.73
667871-6787121.70921.82
45min154245-5424517.35120.069.3317.4920.219.27
262561-6256120.01020.17
363066-6306620.17220.33
461614-6161419.70819.86
562174-6217419.88720.05
672586-7258623.21723.37
60min153062-5306216.97219.9010.1917.1420.0910.13
261082-6108219.53719.73
362667-6266720.04420.24
462021-6202119.83820.03
561482-6148219.66519.86
672940-7294023.33023.52
极限152841-5284116.90119.759.9817.1019.979.90
261649-6164919.71919.95
361049-6104919.52719.75
461406-6140619.64119.86
561276-6127619.59919.83
672201-7220123.09423.32
非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号250201对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
122.107828987822827818307819737797317817430.16
222.147778407807697793040.27
单位质量响应值RSD%判断
35372.9935198.920.35数据可信
供试品溶液-25103101-2-1批-非奈利酮-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min140483-4048310.3266.2536.4410.336.2636.46
224607-246076.2766.28
322548-225485.7515.75
416296-162964.1564.16
526881-268816.8566.86
616327-163274.1644.16
10min166465-6646516.95312.2721.9816.9712.2821.98
250105-5010512.78012.79
346288-4628811.80611.82
437351-373519.5279.53
550051-5005112.76612.78
638377-383779.7889.80
15min183753-8375321.36216.5817.4221.4116.6117.43
269073-6907317.61817.65
363405-6340516.17216.20
452942-5294213.50313.53
566851-6685117.05117.08
653999-5399913.77313.80
20min197469-9746924.86019.9315.6524.9419.9915.67
284159-8415921.46621.53
376859-7685919.60419.66
465290-6529016.65316.70
579907-7990720.38120.44
665189-6518916.62716.67
30min1114081-11408129.09825.0911.7229.2225.1811.75
2106875-10687527.26027.36
398016-9801625.00025.09
485975-8597521.92922.00
5100461-10046125.62425.72
684710-8471021.60621.68
45min1129870-12987033.12529.499.1933.3029.639.22
2123077-12307731.39231.53
3116148-11614829.62529.76
4100199-10019925.55725.67
5116941-11694129.82729.96
6107538-10753827.42927.54
60min1134078-13407834.19832.046.2134.4232.226.25
2131503-13150333.54133.74
3127399-12739932.49432.67
4112725-11272528.75228.90
5127295-12729532.46832.66
6120629-12062930.76830.92
极限1141394-14139436.06435.013.4136.3535.243.45
2142825-14282536.42936.68
3131512-13151233.54433.78
4133138-13313833.95834.16
5139692-13969235.63035.87
6134931-13493134.41634.62
非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号C5654-24-004M2对照品来源中检院对照品使用方法直接使用
对照品含量(%) 98.3对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.103089693075683087683086523085783085070.18
211.173071593071403071500.01
单位质量响应值RSD%判断
27793.4227497.760.76数据可信
供试品溶液-25103101-2-2批-恩格列净-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min150350-5035016.11314.5315.9816.1114.5315.98
249220-4922015.75215.75
333066-3306610.58210.58
452463-5246316.78916.79
546485-4648514.87614.88
640847-4084713.07213.07
10min162304-6230419.93919.946.0819.9719.966.09
267694-6769421.66421.69
362491-6249119.99920.02
462529-6252920.01120.04
562936-6293620.14120.17
655812-5581217.86117.88
15min163033-6303320.17220.142.6120.2320.192.62
264836-6483620.74920.81
362761-6276120.08520.14
463757-6375720.40420.47
563195-6319520.22420.28
659937-5993719.18119.23
20min161285-6128519.61320.083.4019.7120.183.40
265257-6525720.88420.98
363306-6330620.25920.34
463625-6362520.36220.46
563791-6379120.41520.51
659264-5926418.96619.05
30min161225-6122519.59320.091.4019.7220.211.40
263669-6366920.37620.51
363210-6321020.22920.35
462662-6266220.05320.18
563346-6334620.27220.40
662478-6247819.99420.11
45min161631-6163119.72319.760.4919.8819.920.51
262202-6220219.90620.07
361387-6138719.64519.80
461968-6196819.83119.99
561789-6178919.77419.93
661531-6153119.69119.84
60min160193-6019319.26319.561.1819.4619.751.18
262254-6225419.92320.12
360710-6071019.42919.61
461540-6154019.69419.89
560859-6085919.47619.67
661095-6109519.55219.73
极限159536-5953619.05319.391.1019.2819.611.09
261582-6158219.70819.94
360464-6046419.35019.57
460456-6045619.34719.58
560639-6063919.40619.63
660839-6083919.47019.68
非奈利酮恩格列净项目信息
介质体积(ml) 900取样体积(ml)1.5补液体积(ml)1.5
对照品批号250201对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
122.107833337798827827847827777828697823290.18
222.147784857786787785820.02
单位质量响应值RSD%判断
35399.5035166.310.47数据可信
供试品溶液-25103101-2-2批-非奈利酮-pH1.2
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min126624-266246.7915.3626.456.795.3626.44
222346-223465.7005.70
316135-161354.1164.12
423538-235386.0046.00
525143-251436.4146.41
612398-123983.1633.16
10min153380-5338013.61611.6718.1613.6311.6818.16
251281-5128113.08113.09
340560-4056010.34610.35
447337-4733712.07512.08
550454-5045412.87012.88
631451-314518.0238.03
15min171566-7156618.25516.3114.5918.2916.3414.61
271287-7128718.18418.22
358527-5852714.92914.95
466277-6627716.90616.94
568354-6835417.43617.47
647564-4756412.13312.15
20min182870-8287021.13919.7913.3621.2019.8513.38
286654-8665422.10422.17
373126-7312618.65318.70
481113-8111320.69120.75
583271-8327121.24121.30
658553-5855314.93614.97
30min1102898-10289826.24824.9510.3326.3525.0410.35
2105249-10524926.84726.95
395382-9538224.33024.41
4100710-10071025.68925.78
5104155-10415526.56826.66
678476-7847620.01820.08
45min1121137-12113730.90029.419.3931.0429.549.41
2122164-12216431.16231.31
3113672-11367228.99629.12
4119624-11962430.51430.65
5121045-12104530.87731.02
694084-9408423.99924.10
60min1128124-12812432.68232.007.9932.8832.188.01
2132882-13288233.89634.09
3125699-12569932.06432.23
4130566-13056633.30533.49
5129923-12992333.14133.33
6105609-10560926.93927.08
极限1141151-14115136.00535.076.3136.2535.306.34
2144655-14465536.89937.15
3138514-13851435.33335.56
4140725-14072535.89736.14
5139461-13946135.57435.82
6120289-12028930.68430.87
点击查看处理图标(人工保存)
 
原始图谱下载图谱(刘齐慧子 于 2025-11-06 17:01:49 完成)
生成报告数据部分(等待生成报告)
Current page cost:89 ms