富马酸伏诺拉生片片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号17570对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.78对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.7485
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.811247541239431240491218151219061232931.10
214.851232841228041230440.28
单位质量响应值RSD%判断
8324.988285.790.34数据可信
中间条件12月-供试品溶液-2023031211批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1111313-11131390.08887.165.0790.0987.165.07
2114605-11460592.75292.75
3101506-10150682.15182.15
4105797-10579785.62485.62
5111124-11112489.93589.93
6101841-10184182.42282.42
10min1121461-12146198.30197.062.1898.4597.202.19
2123500-12350099.951100.11
3117449-11744995.05495.19
4120708-12070897.69197.83
5119993-11999397.11397.26
6116431-11643194.23094.37
15min1123173-12317399.68698.131.66100.0098.441.67
2123954-123954100.318100.64
3119643-11964396.82997.12
4121658-12165898.46098.77
5120127-12012797.22197.53
6118964-11896496.28096.57
20min1123649-123649100.07298.421.74100.5598.891.75
2124156-124156100.482100.97
3120079-12007997.18297.64
4122389-12238999.05299.52
5120509-12050997.53098.00
6118858-11885896.19496.65
30min1123421-12342199.88799.011.07100.5399.651.07
2124272-124272100.576101.23
3121061-12106197.97798.60
4122266-12226698.95299.59
5122009-12200998.74499.38
6121004-12100497.93198.55
45min1123277-12327799.77199.320.64100.58100.120.65
2123808-123808100.200101.02
3122663-12266399.274100.06
4122600-12260099.223100.02
5122492-12249299.13599.94
6121487-12148798.32299.10
60min1122150-12215098.85898.960.8899.8499.930.89
2123951-123951100.316101.31
3121035-12103597.95698.90
4123083-12308399.614100.58
5121504-12150498.33699.30
6121939-12193998.68899.63
极限1121949-12194998.69698.890.4999.84100.020.50
2123251-12325199.750100.91
3121479-12147998.31599.43
4122320-12232098.996100.13
5121954-12195498.70099.83
6122159-12215998.86699.97
富马酸伏诺拉生片片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号17570对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.78对照品水分(%)0对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数0.7485
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.811227111219881224151225211221061223480.25
214.851224601225761225180.07
单位质量响应值RSD%判断
8261.178250.370.10数据可信
中间条件12月-供试品溶液-2023031311批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1105077-10507785.55287.032.3285.5587.032.32
2108575-10857588.40088.40
3104421-10442185.01785.02
4106359-10635986.59586.60
5105884-10588486.20986.21
6111035-11103590.40290.40
10min1118495-11849596.47697.691.6396.6297.841.63
2119035-11903596.91697.06
3117467-11746795.63995.78
4120780-12078098.33798.48
5121839-12183999.19999.34
6122304-12230499.57799.73
15min1121227-12122798.70199.461.3699.0099.771.36
2120311-12031197.95598.26
3120836-12083698.38298.68
4124599-124599101.446101.75
5122628-12262899.841100.15
6123393-123393100.464100.78
20min1121444-12144498.877100.001.2299.35100.471.22
2121560-12156098.97299.44
3121470-12147098.89899.36
4124723-124723101.547102.02
5123839-123839100.827101.30
6123905-123905100.881101.37
30min1122153-12215399.454100.330.93100.09100.970.93
2122696-12269699.897100.53
3122698-12269899.898100.53
4125420-125420102.114102.76
5123214-123214100.318100.96
6123162-123162100.276100.93
45min1122242-12224299.527100.761.10100.33101.561.09
2123092-123092100.219101.02
3123751-123751100.756101.55
4126254-126254102.793103.61
5123775-123775100.775101.59
6123390-123390100.462101.28
60min1121259-12125998.727100.471.5099.69101.441.49
2122697-12269799.897100.87
3123948-123948100.916101.88
4126565-126565103.047104.03
5123724-123724100.734101.71
6122198-12219899.491100.48
极限1122867-122867100.036100.960.81101.16102.110.81
2122989-122989100.135101.27
3124989-124989101.764102.90
4125164-125164101.906103.07
5124399-124399101.283102.43
6123631-123631100.658101.81
点击查看处理图标(自动生成)
　
原始图谱下载图谱(王丹 于 2024-04-18 15:45:14 完成)
生成报告数据部分(等待生成报告)
Current page cost:69 ms