熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.075381554294539045384453728539170.41
211.195434253799540700.72
单位质量响应值RSD%判断
4870.554831.990.57数据可信
供试品溶液-25102801批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
15min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
20min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
30min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
45min11084-10842.0031.03109.622.001.03109.63
21102-11022.0362.04
31151-11512.1272.13
4-0.0000.00
5-0.0000.00
6-0.0000.00
60min11266-12662.3392.334.112.342.334.07
21243-12432.2972.30
31268-12682.3432.35
41353-13532.5002.50
51233-12332.2782.28
61200-12002.2172.22
极限11586-15862.9313.257.292.943.267.21
21735-17353.2063.21
31698-16983.1383.15
41895-18953.5023.51
51926-19263.5593.56
61719-17193.1763.18
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.075431354105541975458554119542640.37
211.195404953685538670.48
单位质量响应值RSD%判断
4901.904813.851.29数据可信
供试品溶液-25102801批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13549-35496.5496.733.646.556.733.62
23651-36516.7386.74
33625-36256.6906.69
43625-36256.6906.69
53904-39047.2047.20
63540-35406.5336.53
10min14876-48768.9988.365.019.018.375.01
24291-42917.9197.93
34621-46218.5288.54
44370-43708.0648.08
54658-46588.5968.61
64356-43568.0398.05
15min14400-44008.1208.587.108.158.607.06
24495-44958.2958.32
34406-44068.1318.16
44664-46648.6078.63
55281-52819.7469.77
64647-46478.5768.60
20min14175-41757.7058.244.057.748.284.04
24677-46778.6318.67
34425-44258.1668.20
44594-45948.4788.52
54369-43698.0638.11
64546-45468.3898.43
30min14410-44108.1388.064.918.198.114.87
24703-47038.6798.73
34338-43388.0058.06
44436-44368.1868.24
54242-42427.8287.88
64062-40627.4967.55
45min13909-39097.2147.874.837.287.944.80
24509-45098.3218.39
34329-43297.9898.05
44383-43838.0888.16
54287-42877.9117.98
64182-41827.7177.78
60min14009-40097.3987.603.417.487.683.36
24351-43518.0298.11
34123-41237.6097.69
44036-40367.4487.53
53982-39827.3487.43
64199-41997.7497.83
极限13800-38007.0138.099.007.108.188.94
24706-47068.6848.78
34244-42447.8327.92
44928-49289.0949.19
54256-42567.8547.95
64358-43588.0428.13
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