盐酸鲁拉西酮口崩片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号N877-220209对照品来源自制对照品使用方法直接使用
对照品含量(%)99.99对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.141975481980321980841978681980931979250.12
211.112003441998602001020.18
单位质量响应值RSD%判断
17767.0618010.980.97数据可信
供试品溶液-24041201批-pH3.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1143326-14332672.10472.031.6072.1072.031.60
2143522-14352272.20272.20
3144402-14440272.64572.65
4146025-14602573.46273.46
5139169-13916970.01270.01
6142613-14261371.74571.75
10min1167466-16746684.24884.840.8484.3784.960.84
2169587-16958785.31585.44
3170252-17025285.65085.77
4169872-16987285.45885.58
5167159-16715984.09484.21
6167481-16748184.25684.38
15min1177242-17724289.16689.590.7689.4389.850.76
2180180-18018090.64490.91
3178860-17886089.98090.24
4178524-17852489.81190.08
5176965-17696589.02789.28
6176696-17669688.89189.15
20min1181557-18155791.33791.581.2791.7592.001.26
2184868-18486893.00293.42
3184114-18411492.62393.04
4181847-18184791.48391.90
5181550-18155091.33391.74
6178362-17836289.72990.14
30min1188449-18844994.80494.221.2295.3794.781.22
2190089-19008995.62996.20
3188416-18841694.78795.36
4185536-18553693.33993.91
5187433-18743394.29394.85
6183751-18375192.44193.00
45min1190133-19013395.65195.420.8696.3796.140.86
2191596-19159696.38797.12
3190805-19080595.98996.72
4187985-18798594.57195.29
5190028-19002895.59896.31
6187471-18747194.31295.02
60min1194005-19400597.59995.861.1998.4896.741.18
2191381-19138196.27997.17
3190640-19064095.90696.79
4188535-18853594.84795.73
5191059-19105996.11796.99
6187659-18765994.40795.28
极限1191453-19145396.31595.990.8897.3697.030.87
2193699-19369997.44598.49
3190897-19089796.03697.08
4188960-18896095.06196.10
5189991-18999195.58096.61
6189850-18985095.50996.54
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