熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号U202302006对照品来源自制对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.315527454837544335443254465546880.68
211.385596155745558530.28
单位质量响应值RSD%判断
4835.374908.001.06数据可信
供试品溶液-25112101批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min165678-65678121.22096.5716.03121.2296.5716.03
259524-59524109.861109.86
348713-4871389.90889.91
449215-4921590.83490.83
546621-4662186.04786.05
644183-4418381.54781.55
10min159485-59485109.789102.016.63109.99102.176.64
259153-59153109.177109.36
353733-5373399.17399.32
455579-55579102.580102.73
549815-4981591.94292.09
653861-5386199.40999.55
15min158938-58938108.780105.123.47109.16105.453.49
259271-59271109.394109.76
355049-55049101.602101.92
457850-57850106.772107.09
555743-55743102.883103.18
654877-54877101.285101.59
20min159165-59165109.199105.833.04109.77106.343.06
259462-59462109.747110.29
355146-55146101.781102.27
457566-57566106.248106.75
555837-55837103.056103.52
656858-56858104.941105.41
30min159664-59664110.120106.233.15110.87106.913.16
259372-59372109.581110.31
355177-55177101.838102.49
457405-57405105.950106.63
555872-55872103.121103.76
657846-57846106.764107.41
45min159996-59996110.733106.153.35111.66107.013.37
259398-59398109.629110.54
355180-55180101.844102.67
457788-57788106.657107.51
555802-55802102.992103.80
656923-56923105.061105.88
60min158148-58148107.322105.123.06108.44106.163.08
259431-59431109.690110.79
355121-55121101.735102.73
457570-57570106.255107.29
555087-55087101.672102.66
656377-56377104.053105.05
极限159049-59049108.985105.573.22110.28106.783.24
259441-59441109.708110.99
354906-54906101.338102.50
457306-57306105.768106.98
555416-55416102.279103.43
657074-57074105.340106.51
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