布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322747005274568127461982748572274296827460850.08
211.222748792274516827469800.10
单位质量响应值RSD%判断
242587.01244828.880.66数据可信
供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12510381-251038192.61693.931.5592.6293.931.55
22524516-252451693.13893.14
32574813-257481394.99394.99
42608779-260877996.24696.25
52510685-251068592.62792.63
62546937-254693793.96593.96
10min12568003-256800394.74294.901.0795.2695.421.07
22549738-254973894.06894.59
32614115-261411596.44396.97
42591129-259112995.59596.13
52538280-253828093.64694.16
62572619-257261994.91295.43
15min12556461-255646194.31694.591.6495.3695.641.63
22545925-254592593.92894.97
32634032-263403297.17898.24
42588952-258895295.51596.58
52515255-251525592.79693.83
62542168-254216893.78994.84
20min12524469-252446993.13694.031.2194.7095.601.21
22524571-252457193.14094.70
32595285-259528595.74997.35
42579490-257949095.16696.76
52533298-253329893.46295.01
62534322-253432293.50095.07
30min12520566-252056692.99293.601.3195.0795.701.31
22530078-253007893.34395.42
32579598-257959895.17097.31
42575592-257559295.02297.15
52497945-249794592.15794.23
62518333-251833392.91095.00
极限12512526-251252692.69593.001.1695.2995.621.16
22509637-250963792.58995.19
32562738-256273894.54897.21
42545128-254512893.89896.55
52480290-248029091.50694.09
62514430-251443092.76695.37
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322743811274934527480672746432274515127465610.09
211.222738868274550227421850.18
单位质量响应值RSD%判断
242629.06244401.520.52数据可信
供试品溶液-2025103151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12535463-253546393.61594.371.2493.6194.371.24
22539041-253904193.74793.75
32522102-252210293.12293.12
42564731-256473194.69594.70
52564092-256409294.67294.67
62610519-261051996.38696.39
10min12556320-255632094.38595.471.0494.9195.991.04
22580702-258070295.28595.81
32557932-255793294.44494.96
42596278-259627895.86096.39
52594744-259474495.80496.33
62627668-262766897.01997.55
15min12538545-253854593.72994.901.2194.7795.951.21
22550672-255067294.17695.23
32544090-254409093.93394.98
42583697-258369795.39696.45
52585573-258557395.46596.52
62618488-261848896.68097.75
20min12511269-251126992.72293.981.6394.2995.571.62
22526221-252622193.27494.85
32495024-249502492.12293.69
42570010-257001094.89096.48
52566022-256602294.74396.33
62604239-260423996.15497.77
30min12511012-251101292.71293.601.1094.7995.701.10
22517967-251796792.96995.06
32504932-250493292.48894.56
42550465-255046594.16996.28
52552066-255206694.22896.34
62574184-257418495.04597.19
极限12481347-248134791.61792.981.3394.2195.601.33
22509247-250924792.64795.25
32489591-248959191.92194.51
42519116-251911693.01195.65
52537450-253745093.68896.33
62572552-257255294.98497.66
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322747794274054727487732750920274634527468760.15
211.222741666274599027438280.12
单位质量响应值RSD%判断
242656.89244547.950.55数据可信
供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12496539-249653992.14593.591.1592.1493.591.16
22530535-253053593.40093.40
32508776-250877692.59792.60
42553828-255382894.25994.26
52551755-255175594.18394.18
62572799-257279994.96094.96
10min12564755-256475594.66395.500.8695.1796.020.86
22589532-258953295.57796.10
32558213-255821394.42194.94
42615843-261584396.54897.07
52602972-260297296.07396.60
62592705-259270595.69496.22
15min12548456-254845694.06195.060.9095.1096.120.90
22574604-257460495.02696.08
32554120-255412094.27095.31
42612363-261236396.42097.48
52586223-258622395.45596.51
62577960-257796095.15096.21
20min12533753-253375393.51894.401.0695.0895.981.06
22557578-255757894.39895.98
32519990-251999093.01094.57
42593904-259390495.73997.33
52567190-256719094.75396.34
62573095-257309594.97196.56
30min12540863-254086393.78194.431.0195.8696.531.01
22533609-253360993.51395.62
32542094-254209493.82695.91
42603594-260359496.09698.22
52564290-256429094.64696.76
62566130-256613094.71396.83
极限12517790-251779092.92993.821.1095.5396.451.10
22540381-254038193.76396.38
32506642-250664292.51895.12
42580046-258004695.22797.89
52540145-254014593.75496.39
62566447-256644794.72597.37
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322742909274036527442762740523274309527422340.07
211.222746662273979627432290.18
单位质量响应值RSD%判断
242246.82244494.560.66数据可信
供试品溶液-2025110151批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12490515-249051592.01193.831.5892.0193.831.58
22539854-253985493.83393.83
32517308-251730893.00193.00
42529338-252933893.44593.44
52553532-255353294.33994.34
62608529-260852996.37196.37
10min12538391-253839193.77995.351.4894.2995.871.49
22582523-258252395.41095.93
32558288-255828894.51495.03
42558794-255879494.53395.05
52602993-260299396.16696.69
62644050-264405097.68398.22
15min12527442-252744293.37594.671.3694.4195.721.36
22563719-256371994.71595.77
32550510-255051094.22795.27
42529231-252923193.44194.49
52588565-258856595.63396.69
62615820-261582096.64097.72
20min12513443-251344392.85894.051.2894.4195.631.28
22554930-255493094.39095.97
32516544-251654492.97294.54
42536206-253620693.69995.26
52551022-255102294.24695.84
62602220-260222096.13897.75
30min12501187-250118792.40593.901.4894.4796.001.48
22546811-254681194.09096.19
32511539-251153992.78794.87
42542250-254225093.92296.01
52540297-254029793.85095.96
62608647-260864796.37598.52
极限12480477-248047791.64093.411.6494.2296.031.63
22533314-253331493.59296.22
32501112-250111292.40295.00
42518022-251802293.02795.63
52536047-253604793.69396.33
62601219-260121996.10198.79
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