布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322674621267762026751102675863267864526763720.07
211.222678463267908626787740.02
单位质量响应值RSD%判断
236428.62238749.910.70数据可信
供试品溶液-241116464批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12481792-248179293.92093.281.2593.9293.281.25
22475133-247513393.66893.67
32493249-249324994.35394.35
42486869-248686994.11294.11
52426410-242641091.82491.82
62425630-242563091.79491.79
10min12563798-256379897.02396.381.1197.5496.901.11
22566662-256666297.13297.65
32574392-257439297.42497.95
42552468-255246896.59497.12
52508870-250887094.94495.45
62515024-251502495.17795.69
15min12578780-257878097.59097.050.6698.6598.100.66
22575863-257586397.48098.54
32578103-257810397.56498.63
42566003-256600397.10798.17
52539902-253990296.11997.16
62547718-254771896.41597.45
20min12568823-256882397.21396.530.6798.8298.120.68
22557905-255790596.80098.40
32566139-256613997.11298.72
42550750-255075096.52998.13
52530162-253016295.75097.32
62530951-253095195.78097.35
30min12552301-255230196.58895.980.5498.7398.110.55
22536857-253685796.00498.14
32547864-254786496.42098.57
42539856-253985696.11798.25
52518594-251859495.31297.42
62522092-252209295.44597.55
极限12622324-262232499.23896.001.77101.9298.661.74
22526663-252666395.61898.29
32544776-254477696.30398.99
42520624-252062495.38998.06
52499649-249964994.59697.23
62506834-250683494.86797.50
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322682903268174026822972681298268207126820620.03
211.222679847267890926793780.03
单位质量响应值RSD%判断
236931.27238803.740.56数据可信
供试品溶液-241116464批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12369407-236940789.56193.752.6089.5693.752.60
22484716-248471693.92093.92
32496747-249674794.37494.37
42455443-245544392.81392.81
52559080-255908096.73196.73
62516719-251671995.12995.13
10min12501982-250198294.57296.501.5895.0797.021.59
22564207-256420796.92497.45
32564401-256440196.93297.46
42511426-251142694.92995.44
52610928-261092898.69099.23
62565244-256524496.96497.49
15min12529328-252932895.60697.543.1896.6398.593.16
22577955-257795597.44498.50
32563504-256350496.89897.96
42515953-251595395.10096.14
52741217-2741217103.615104.70
62554582-255458296.56097.63
20min12519215-251921595.22496.161.1396.7897.761.14
22566746-256674697.02098.62
32544803-254480396.19197.79
42508486-250848694.81896.39
52584748-258474897.70199.36
62540013-254001396.01097.61
30min12502586-250258694.59595.651.3596.6897.781.36
22556771-255677196.64398.78
32531793-253179395.69997.83
42484359-248435993.90696.00
52577422-257742297.42499.63
62530287-253028795.64297.78
极限12486948-248694894.00495.121.2896.6197.791.29
22536031-253603195.85998.54
32515096-251509695.06897.74
42477236-247723693.63796.26
52564488-256448896.93599.68
62519432-251943295.23297.90
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322676757267802726794702678322268093526787020.06
211.222677450267996426787070.07
单位质量响应值RSD%判断
236634.45238743.940.63数据可信
供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12517496-251749695.23094.870.9395.2394.870.93
22504564-250456494.74194.74
32483810-248381093.95693.96
42545775-254577596.30096.30
52483861-248386193.95893.96
62512718-251271895.05095.05
10min12558886-255888696.79696.861.0797.3397.391.06
22558138-255813896.76897.29
32529258-252925895.67596.20
42602030-260203098.42898.96
52535550-253555095.91396.44
62579686-257968697.58398.11
15min12551036-255103696.49996.821.1797.5797.881.16
22565234-256523497.03698.10
32527021-252702195.59196.64
42601205-260120598.39799.48
52528864-252886495.66096.72
62583492-258349297.72798.80
20min12537953-253795396.00496.281.1597.6197.891.15
22546283-254628396.31997.92
32519961-251996195.32496.91
42593361-259336198.10099.73
52513485-251348595.07996.67
62561130-256113096.88198.49
30min12522661-252266195.42695.941.6797.5698.081.66
22536652-253665295.95598.09
32498474-249847494.51196.63
42610497-261049798.748100.92
52496914-249691494.45296.57
62552491-255249196.55498.71
极限12510292-251029294.95895.161.0897.6297.831.08
22514713-251471395.12597.80
32490907-249090794.22596.86
42557941-255794196.76099.48
52485973-248597394.03896.68
62533555-253355595.83898.53
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322680825267975726800842681314267797426799910.05
211.222686619268573726861780.03
单位质量响应值RSD%判断
236748.32239409.800.80数据可信
供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12499366-249936694.39194.831.7994.3994.831.80
22443031-244303192.26392.26
32513079-251307994.90994.91
42509738-250973894.78394.78
52517030-251703095.05895.06
62583725-258372597.57797.58
10min12607155-260715598.46297.071.1998.9997.601.19
22519464-251946495.15095.66
32560515-256051596.70097.23
42565703-256570396.89697.42
52575323-257532397.26097.79
62593691-259369197.95398.50
15min12556225-255622596.53896.700.7397.6197.770.73
22528251-252825195.48296.52
32559434-255943496.65997.72
42564138-256413896.83797.90
52573023-257302397.17398.24
62582444-258244497.52898.61
20min12530355-253035595.56196.200.7597.1797.810.76
22524011-252401195.32296.89
32547341-254734196.20397.80
42545851-254585196.14697.75
52561258-256125896.72898.34
62575338-257533897.26098.89
30min12535419-253541995.75295.660.8597.8997.790.85
22498180-249818094.34696.45
32526796-252679695.42797.56
42527544-252754495.45597.59
52548924-254892496.26398.41
62560371-256037196.69598.86
极限12508469-250846994.73595.060.7197.4197.730.72
22488903-248890393.99696.62
32513511-251351194.92597.59
42521464-252146495.22597.89
52529894-252989495.54498.22
62540117-254011795.93098.64
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