布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322726507274186127349122736471273980427359110.22
211.222731480272166127265700.26
单位质量响应值RSD%判断
241688.25243009.800.39数据可信
供试品溶液-240920336批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12450423-245042390.91092.201.1590.9192.201.16
22449459-244945990.87490.87
32505676-250567692.96092.96
42492506-249250692.47192.47
52497166-249716692.64492.64
62516387-251638793.35793.36
10min12507017-250701793.00994.831.0293.5195.341.02
22558639-255863994.92595.43
32579747-257974795.70896.22
42564253-256425395.13395.65
52552950-255295094.71495.23
62573827-257382795.48896.01
15min12517656-251765693.40494.990.9994.4396.040.99
22552539-255253994.69895.73
32578203-257820395.65096.70
42568061-256806195.27496.32
52556290-255629094.83795.88
62590333-259033396.10097.15
20min12509957-250995793.11994.480.7394.6696.040.74
22545791-254579194.44896.01
32551098-255109894.64596.22
42558238-255823894.91096.48
52556881-255688194.85996.43
62557674-255767494.88996.47
30min12507089-250708993.01294.270.7795.0796.360.77
22543863-254386394.37696.46
32550798-255079894.63496.74
42535970-253597094.08496.18
52543100-254310094.34896.44
62565542-256554295.18197.29
极限12490877-249087792.41193.670.6994.9996.280.69
22523932-252393293.63796.24
32537565-253756594.14396.77
42530963-253096393.89896.52
52529825-252982593.85696.47
62535241-253524194.05796.70
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.322728988273524927208002740272273489427320410.28
211.222722164272877327254680.18
单位质量响应值RSD%判断
241346.38242911.590.46数据可信
供试品溶液-240920336批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12536361-253636194.18494.091.6894.1894.091.68
22566243-256624395.29495.29
32462193-246219391.43091.43
42534511-253451194.11594.12
52518835-251883593.53393.53
62585217-258521795.99896.00
10min12607365-260736596.82196.761.7497.3497.281.74
22627835-262783597.58198.11
32524540-252454093.74594.25
42596853-259685396.43096.95
52659673-265967398.76399.28
62618687-261868797.24197.77
15min12604182-260418296.70295.931.5097.7696.991.50
22608314-260831496.85697.93
32514882-251488293.38694.42
42577819-257781995.72396.78
52572152-257215295.51396.58
62622779-262277997.39398.47
20min12600061-260006196.54995.741.3598.1597.341.36
22592779-259277996.27997.89
32517303-251730393.47695.02
42572422-257242295.52397.11
52569955-256995595.43197.03
62617550-261755097.19998.81
30min12566362-256636295.29894.851.5997.4396.981.58
22577487-257748795.71197.86
32481867-248186792.16094.23
42560222-256022295.07097.19
52540612-254061294.34296.47
62599249-259924996.51998.67
极限12572038-257203895.50994.671.4698.1797.321.46
22577296-257729695.70498.38
32479859-247985992.08694.66
42535052-253505294.13596.78
52564161-256416195.21697.87
62568799-256879995.38898.08
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