布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972666749265519326585682668973266049326619950.22
211.072673420267103126722260.07
单位质量响应值RSD%判断
242661.35241393.500.38数据可信
供试品溶液-2025110251批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1981024-98102436.44440.346.3236.4440.346.32
21094411-109441140.65640.66
31094296-109429640.65240.65
41038929-103892938.59538.60
51131732-113173242.04342.04
61175629-117562943.67343.67
10min11203947-120394744.72543.823.1544.9344.053.13
21189383-118938344.18444.41
31234775-123477545.87146.10
41134083-113408342.13042.34
51150325-115032542.73342.97
61165447-116544743.29543.54
15min11187707-118770744.12245.253.0644.5745.723.04
21212315-121231545.03645.51
31187932-118793244.13044.61
41193695-119369544.34544.79
51275912-127591247.39947.87
61251399-125139946.48846.97
20min11294592-129459248.09349.093.0048.7949.812.99
21289625-128962547.90848.63
31305253-130525348.48949.21
41295287-129528748.11948.81
51377255-137725551.16451.90
61366337-136633750.75851.50
30min11382790-138279051.36950.742.1952.3351.732.12
21404789-140478952.18653.17
31350138-135013850.15651.15
41377182-137718251.16152.12
51362330-136233050.60951.63
61318071-131807148.96549.99
45min11383251-138325151.38646.787.6652.6348.057.45
21373092-137309251.00952.29
31238611-123861146.01347.29
41168144-116814443.39544.64
51169457-116945743.44444.74
61222411-122241145.41146.71
60min11262683-126268346.90747.645.7848.4449.175.63
21239565-123956546.04947.61
31335044-133504449.59551.12
41169992-116999243.46444.95
51309373-130937348.64250.18
61377698-137769851.18052.73
极限11234996-123499645.87948.896.0447.6750.685.80
21397491-139749151.91553.73
31270576-127057647.20149.01
41426868-142686853.00754.74
51252875-125287546.54348.35
61312703-131270348.76650.60
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972667033265920826714372670131267348726682590.21
211.072671938267461826732780.08
单位质量响应值RSD%判断
243232.36241488.530.51数据可信
供试品溶液-2025110251批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1999590-99959037.08337.874.1137.0837.874.11
2994885-99488536.90836.91
3974503-97450336.15236.15
41068485-106848539.63939.64
51076745-107674539.94539.95
61010676-101067637.49437.49
10min11200752-120075244.54641.713.9044.7541.923.89
21089013-108901340.40040.61
31086029-108602940.29040.49
41119458-111945841.53041.75
51147756-114775642.58042.80
61102577-110257740.90441.11
15min11190471-119047144.16443.633.7344.6244.083.70
21155116-115511642.85343.28
31214500-121450045.05645.48
41193713-119371344.28544.74
51205911-120591144.73745.20
61096900-109690040.69341.13
20min11205338-120533844.71643.732.0945.4144.422.08
21161276-116127643.08143.75
31183724-118372443.91444.59
41156000-115600042.88543.58
51210013-121001344.88945.60
61156803-115680342.91543.58
30min11179906-117990643.77245.115.2744.7246.035.20
21153229-115322942.78343.69
31240079-124007946.00546.92
41199425-119942544.49645.43
51333078-133307849.45550.41
61189335-118933544.12245.02
45min11384670-138467051.36946.418.1052.5647.597.94
21226896-122689645.51646.66
31176178-117617843.63444.81
41302664-130266448.32649.51
51310005-131000548.59949.83
61105900-110590041.02742.17
60min11198263-119826344.45346.085.2045.9347.525.02
21248549-124854946.31947.72
31141286-114128642.34043.76
41309534-130953448.58150.03
51248852-124885246.33047.83
61306151-130615148.45649.83
极限11264830-126483046.92347.745.4448.6549.445.27
21166619-116661943.27944.93
31290467-129046747.87449.53
41322072-132207249.04650.77
51300846-130084648.25950.02
61376756-137675651.07552.72
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