布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972635349263391226339202635788263179926341540.06
211.072622460262105926217600.04
单位质量响应值RSD%判断
240123.43236834.690.98数据可信
供试品溶液-241116464批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12445770-244577092.21392.801.0192.2192.801.01
22452524-245252492.46892.47
32494920-249492094.06794.07
42489565-248956593.86593.86
52436021-243602191.84691.85
62448480-244848092.31692.32
10min12467669-246766993.03994.100.9793.5594.620.97
22498490-249849094.20194.71
32524431-252443195.17995.70
42519547-251954794.99595.52
52468886-246888693.08593.60
62495925-249592594.10494.62
15min12500675-250067594.28395.290.7995.3196.330.79
22522877-252287795.12196.16
32553557-255355796.27797.33
42547914-254791496.06597.11
52520583-252058395.03496.06
62518438-251843894.95395.99
20min12506914-250691494.51995.280.6696.0796.850.66
22538103-253810395.69597.26
32547264-254726496.04097.63
42537199-253719995.66197.24
52508828-250882894.59196.15
62524753-252475395.19196.75
30min12510651-251065194.66094.890.5896.7496.990.58
22526062-252606295.24197.34
32531507-253150795.44697.57
42528736-252873695.34197.46
52493802-249380294.02496.11
62510420-251042094.65196.74
45min12497558-249755894.16694.320.4796.7796.940.47
22502923-250292394.36896.99
32516622-251662294.88597.53
42512747-251274794.73997.38
52486273-248627393.74096.34
62493181-249318194.00196.62
60min12484261-248426193.66593.730.4896.7996.880.49
22491355-249135593.93297.08
32499883-249988394.25497.43
42495911-249591194.10497.27
52469271-246927193.09996.22
62475721-247572193.34396.48
极限12468174-246817493.05893.270.5896.7196.940.58
22477703-247770393.41797.09
32487788-248778893.79897.50
42490401-249040193.89697.59
52452525-245252592.46896.11
62466847-246684793.00896.67
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972623135262842526293572626151262697426268080.10
211.072621933262254526222390.02
单位质量响应值RSD%判断
239453.78236877.960.77数据可信
供试品溶液-241116464批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12445680-244568092.33093.521.9692.3393.521.97
22411091-241109191.02491.02
32462483-246248392.96492.96
42478800-247880093.58093.58
52540188-254018895.89795.90
62524320-252432095.29895.30
10min12483028-248302893.74095.221.6794.2595.741.68
22479548-247954893.60894.11
32497779-249777994.29694.81
42531508-253150895.57096.09
52563502-256350296.77897.31
62577916-257791697.32297.85
15min12536173-253617395.74696.150.8796.7897.190.88
22522820-252282095.24296.27
32529253-252925395.48596.52
42545871-254587196.11297.16
52568650-256865096.97298.04
62577795-257779597.31798.39
20min12535838-253583895.73396.140.6597.3097.730.66
22523518-252351895.26896.82
32543064-254306496.00697.58
42548275-254827596.20397.79
52562254-256225496.73098.34
62567459-256745996.92798.54
30min12524444-252444495.30395.590.6697.4097.710.67
22504872-250487294.56496.65
32536153-253615395.74597.85
42530134-253013495.51897.64
52545169-254516996.08598.23
62551637-255163796.33098.48
45min12516549-251654995.00595.000.5297.6397.650.54
22492043-249204394.08096.69
32517797-251779795.05297.69
42517421-251742195.03897.69
52526537-252653795.38298.06
62528757-252875795.46698.15
60min12494905-249490594.18894.440.7397.3497.620.74
22472595-247259593.34696.48
32503634-250363494.51797.68
42500421-250042194.39697.57
52511265-251126594.80698.02
62527427-252742795.41698.63
极限12480029-248002993.62693.980.6897.3097.680.70
22462656-246265692.97096.62
32487128-248712893.89497.58
42494408-249440894.16997.87
52503678-250367894.51998.26
62509141-250914194.72598.47
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972623516262196626218882621832262307026224540.03
211.072627217262744126273290.01
单位质量响应值RSD%判断
239056.88237337.760.52数据可信
供试品溶液-250226083批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12407692-240769290.88290.740.6690.8890.740.65
22383830-238383089.98189.98
32416112-241611291.20091.20
42426037-242603791.57491.57
52396649-239664990.46590.47
62392991-239299190.32790.33
10min12448594-244859492.42693.091.1892.9393.601.18
22443216-244321692.22392.72
32465643-246564393.06993.58
42517671-251767195.03395.54
52442951-244295192.21392.72
62479360-247936093.58794.09
15min12486332-248633293.85094.021.2394.8795.041.23
22482198-248219893.69494.71
32467467-246746793.13894.16
42540106-254010695.88096.92
52456571-245657192.72793.74
62511774-251177494.81195.83
20min12480548-248054893.63293.811.1895.1795.361.18
22493611-249361194.12595.66
32466990-246699093.12094.66
42524439-252443995.28996.86
52441342-244134292.15293.68
62505029-250502994.55696.10
30min12470257-247025793.24493.261.1095.3095.321.10
22475079-247507993.42695.48
32451428-245142892.53394.59
42511335-251133594.79496.89
52432272-243227291.81093.85
62483802-248380293.75595.83
45min12449390-244939092.45692.701.1995.0395.281.19
22458758-245875892.81095.38
32441036-244103692.14194.71
42495513-249551394.19796.82
52412026-241202691.04693.60
62478340-247834093.54996.14
60min12438248-243824892.03592.341.2195.1395.431.20
22454608-245460892.65395.74
32427599-242759991.63394.72
42490416-249041694.00597.15
52405010-240501090.78193.84
62461388-246138892.90996.02
极限12425515-242551591.55591.741.1095.1695.351.10
22444026-244402692.25395.86
32415971-241597191.19494.79
42465440-246544093.06296.73
52388625-238862590.16293.72
62443053-244305392.21795.85
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972630031263010826283052623146262642726276030.12
211.072629704262946026295820.01
单位质量响应值RSD%判断
239526.25237541.280.59数据可信
供试品溶液-250226083批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12427900-242790091.51691.782.2291.5291.782.22
22362918-236291889.06689.07
32446333-244633392.21192.21
42409746-240974690.83290.83
52434778-243477891.77591.78
62527559-252755995.27295.27
10min12482467-248246793.57393.871.5194.0894.381.52
22437740-243774091.88792.38
32505672-250567294.44794.96
42465508-246550892.93393.44
52502967-250296794.34594.86
62547125-254712596.01096.54
15min12484906-248490693.66594.291.0794.6995.321.08
22483633-248363393.61794.62
32515403-251540394.81495.85
42474016-247401693.25494.28
52504462-250446294.40295.44
62546554-254655495.98897.05
20min12469458-246945893.08293.761.0594.6395.311.05
22476569-247656993.35094.88
32497684-249768494.14695.71
42457934-245793492.64894.19
52490607-249060793.88095.44
62531594-253159495.42497.02
30min12452064-245206492.42793.071.0294.4995.151.03
22455432-245543292.55494.60
32480102-248010293.48495.57
42442303-244230392.05994.11
52473112-247311293.22095.30
62511841-251184194.68096.81
45min12442138-244213892.05392.681.0794.6395.271.08
22448007-244800792.27494.83
32469854-246985493.09795.70
42426996-242699691.48294.05
52463572-246357292.86095.46
62502240-250224094.31896.97
60min12425823-242582391.43892.041.0294.5395.151.03
22433611-243361191.73194.80
32446388-244638892.21395.34
42416345-241634591.08094.15
52441014-244101492.01095.12
62487521-248752193.76396.94
极限12412635-241263590.94091.630.9794.5495.240.98
22423193-242319391.33894.92
32441934-244193492.04595.68
42403908-240390890.61294.19
52433258-243325891.71895.34
62469958-246995893.10196.80
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