布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972666659268084626738642682052268279826772440.26
211.072673232266619926697160.19
单位质量响应值RSD%判断
244051.41241166.760.85数据可信
供试品溶液-240920336批-pH6.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12265588-226558883.96585.253.4783.9685.253.47
22188123-218812381.09481.09
32246537-224653783.25983.26
42341850-234185086.79186.79
52362417-236241787.55387.55
62397835-239783588.86688.87
10min12362236-236223687.54788.413.1988.0188.883.19
22277555-227755584.40884.86
32329474-232947486.33286.80
42422581-242258189.78390.27
52439317-243931790.40390.89
62481503-248150391.96792.46
15min12378857-237885788.16388.883.0289.1289.853.02
22292329-229232984.95685.88
32346421-234642186.96187.90
42438794-243879490.38491.36
52446330-244633090.66391.65
62487023-248702392.17193.18
20min12386598-238659888.45088.903.2289.8990.363.22
22277454-227745484.40585.80
32349710-234971087.08288.51
42440071-244007190.43191.91
52449051-244905190.76492.26
62489375-248937592.25993.78
30min12401181-240118188.99088.762.8890.9290.722.88
22287639-228763984.78286.64
32338211-233821186.65688.57
42440508-244050890.44792.43
52437366-243736690.33192.33
62465631-246563191.37993.41
45min12402537-240253789.04088.992.5991.4791.442.60
22307706-230770685.52687.86
32350248-235024887.10289.49
42438099-243809990.35892.85
52432513-243251390.15192.65
62475620-247562091.74994.29
60min12411399-241139989.36989.262.3992.2992.202.40
22300266-230026685.25088.06
32403417-240341789.07391.95
42433695-243369590.19593.18
52436156-243615690.28693.29
62465907-246590791.38994.44
极限12507276-250727692.92291.391.7896.3494.821.81
22397736-239773688.86292.14
32424519-242451989.85593.22
42491486-249148692.33795.83
52486015-248601592.13495.63
62488196-248819692.21595.77
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.972684811268316226674652664778267030926741050.35
211.072686045267868126823630.20
单位质量响应值RSD%判断
243765.27242309.210.43数据可信
供试品溶液-240920336批-pH6.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12270867-227086784.01085.702.8284.0185.702.82
22261198-226119883.65283.65
32301567-230156785.14685.15
42285888-228588884.56684.57
52344112-234411286.72086.72
62435663-243566390.10790.11
10min12336485-233648586.43788.502.9186.9088.972.91
22335244-233524486.39286.86
32384107-238410788.19988.67
42354199-235419987.09387.56
52428665-242866589.84890.33
62514413-251441393.02093.52
15min12360422-236042287.32388.592.4988.2789.562.49
22365486-236548687.51088.46
32375932-237593287.89788.86
42346761-234676186.81887.77
52412618-241261889.25490.23
62507352-250735292.75993.78
20min12363601-236360187.44188.722.4088.8790.182.40
22374866-237486687.85789.29
32382198-238219888.12989.58
42342428-234242886.65788.09
52425035-242503589.71391.19
62501308-250130892.53594.07
30min12371521-237152187.73488.872.4189.6590.822.41
22377755-237775587.96489.88
32390733-239073388.44490.39
42344989-234498986.75288.67
52419312-241931289.50291.48
62509060-250906092.82294.87
45min12375769-237576987.89189.062.0990.3091.502.10
22384495-238449588.21490.62
32394096-239409688.56991.00
42363902-236390287.45289.85
52424418-242441889.69192.16
62500763-250076392.51595.08
60min12363637-236363787.44289.112.1690.3492.052.16
22371102-237110287.71890.62
32401709-240170988.85091.77
42373551-237355187.80990.69
52451244-245124490.68393.65
62491625-249162592.17795.25
极限12459662-245966290.99492.711.6294.3796.151.63
22494325-249432592.27795.66
32493351-249335192.24195.66
42478976-247897691.70995.08
52564688-256468894.88098.35
62545841-254584194.18397.77
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