左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.718543185923857248590585922857810.25
213.778664486449865460.16
单位质量响应值RSD%判断
6256.826285.110.32数据可信
供试品溶液-2024031813批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min179781-7978188.53090.121.7288.5390.121.72
281477-8147790.41290.41
383141-8314192.25892.26
482170-8217091.18191.18
581205-8120590.11090.11
679483-7948388.19988.20
10min186607-8660796.10495.470.9996.9996.380.98
286997-8699796.53797.44
386329-8632995.79696.72
484682-8468293.96894.88
586215-8621595.66996.57
685399-8539994.76495.65
15min185590-8559094.97694.321.2796.8296.171.25
285572-8557294.95696.83
384893-8489394.20396.08
485566-8556694.94996.80
585475-8547594.84896.71
682871-8287191.95993.79
20min183450-8345092.60192.601.2395.4095.401.19
284010-8401093.22396.04
382030-8203091.02693.85
483005-8300592.10794.91
585056-8505694.38397.19
683162-8316292.28295.03
30min179670-7967088.40789.262.2592.1392.982.17
282675-8267591.74195.49
380329-8032989.13892.87
477418-7741885.90889.63
581563-8156390.50794.26
680973-8097389.85393.52
45min180436-8043689.25788.241.0593.8692.861.02
279664-7966488.40093.07
378911-7891187.56592.19
479204-7920487.89092.47
580480-8048089.30693.96
678424-7842487.02491.59
60min178817-7881787.46086.511.3592.9692.011.29
277201-7720185.66791.22
377789-7778986.31991.82
476803-7680385.22590.69
579581-7958188.30893.86
677564-7756486.07091.51
极限177727-7772786.25185.041.5592.6291.401.44
276697-7669785.10891.52
375970-7597084.30190.66
474944-7494483.16289.47
576283-7628384.64891.08
678171-7817186.74393.04
左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202406对照品来源中检院对照品使用方法直接使用
对照品含量(%)96.5对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.718649086479865018670786707865770.14
213.778688886949869180.05
单位质量响应值RSD%判断
6314.886312.130.04数据可信
供试品溶液-2024031813批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min177628-7762885.56085.044.0785.5685.044.07
278816-7881686.86986.87
371766-7176679.09979.10
479803-7980387.95787.96
579676-7967687.81787.82
675222-7522282.90882.91
10min184090-8409092.68292.320.5893.5493.180.56
283184-8318491.68492.55
384468-8446893.09993.89
483651-8365192.19893.08
583869-8386992.43993.32
683325-8332591.83992.67
15min183517-8351792.05190.910.7993.8392.680.76
281521-8152189.85191.64
382557-8255790.99392.71
482272-8227290.67992.48
582359-8235990.77492.58
682646-8264691.09192.84
20min182191-8219190.58989.431.2993.2992.121.24
281651-8165189.99492.68
381252-8125289.55492.19
480359-8035988.57091.28
579459-7945987.57890.29
681941-8194190.31492.97
30min180186-8018688.37988.280.4891.9991.850.45
279848-7984888.00791.59
380198-8019888.39391.92
479525-7952587.65191.24
580134-8013488.32291.91
680663-8066388.90592.47
45min178725-7872586.76986.431.1791.2690.881.10
279096-7909687.17891.64
379205-7920587.29891.71
476756-7675684.59989.07
578682-7868286.72291.19
678015-7801585.98790.44
60min177426-7742685.33784.691.0890.7090.011.01
277087-7708784.96490.30
378000-7800085.97091.25
475735-7573583.47488.79
576411-7641184.21989.56
676355-7635584.15789.47
极限176884-7688484.74083.801.1590.9589.971.09
276345-7634584.14690.33
375792-7579283.53689.68
474556-7455682.17488.33
575755-7575583.49689.67
676859-7685984.71290.86
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