布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.022680124268135926857082672829267355826787160.21
210.972673492267111626723040.07
单位质量响应值RSD%判断
243077.68243601.090.16数据可信
供试品溶液-241116464批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11041941-104194138.49837.084.3038.5037.084.30
21050295-105029538.80738.81
31017279-101727937.58737.59
41006575-100657537.19137.19
5964945-96494535.65335.65
6940674-94067434.75634.76
10min11239844-123984445.81045.991.7046.0246.201.70
21277414-127741447.19847.41
31253582-125358246.31846.53
41249720-124972046.17546.38
51232544-123254445.54145.74
61215026-121502644.89345.09
15min11367926-136792650.54349.713.1551.0150.173.12
21261944-126194446.62747.10
31374652-137465250.79151.26
41370044-137004450.62151.08
51344985-134498549.69550.15
61352002-135200249.95450.40
20min11430186-143018652.84352.565.0853.5953.305.02
21478053-147805354.61255.35
31445147-144514753.39654.14
41476403-147640354.55155.30
51282873-128287347.40048.13
61422162-142216252.54753.27
30min11478616-147861654.63351.485.3155.6852.515.18
21351936-135193649.95250.99
31332698-133269849.24150.29
41345044-134504449.69750.74
51497226-149722655.32056.31
61354782-135478250.05751.07
45min11362772-136277250.35256.435.5151.7057.755.37
21596258-159625858.97960.30
31557357-155735757.54258.86
41564477-156447757.80559.13
51562543-156254357.73459.03
61520425-152042556.17757.47
60min11550157-155015757.27655.315.8558.9056.945.69
21410986-141098652.13453.78
31587531-158753158.65760.29
41526901-152690156.41758.06
51540021-154002156.90158.52
61366388-136638850.48652.09
极限11473322-147332254.43756.125.0356.3858.064.88
21470178-147017854.32156.26
31651712-165171261.02862.99
41458429-145842953.88755.84
51569738-156973857.99959.93
61489765-148976555.04456.93
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.022676556267466626789182671914267757926759270.11
210.972672690267809626753930.15
单位质量响应值RSD%判断
242824.59243882.680.31数据可信
供试品溶液-241116464批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1965727-96572735.68038.106.0635.6838.106.07
21088517-108851740.21740.22
31077055-107705539.79339.79
4939548-93954834.71334.71
51055230-105523038.98738.99
61060470-106047039.18139.18
10min11301247-130124748.07647.151.4648.2747.361.45
21272130-127213047.00147.22
31295852-129585247.87748.10
41259764-125976446.54446.74
51255845-125584546.39946.62
61272473-127247347.01347.23
15min11410312-141031252.10651.500.9152.5751.980.92
21392701-139270151.45551.94
31394975-139497551.53952.03
41372459-137245950.70751.16
51391585-139158551.41451.89
61401954-140195451.79752.28
20min11457270-145727053.84152.576.3154.6053.336.25
21461238-146123853.98754.76
31482925-148292554.78955.56
41241586-124158645.87246.61
51444242-144424253.36054.12
61449515-144951553.55454.32
30min11520431-152043156.17455.552.6057.2356.602.55
21528796-152879656.48457.55
31518707-151870756.11157.19
41524927-152492756.34157.33
51426070-142607052.68853.74
61502886-150288655.52656.59
45min11578430-157843058.31757.371.6959.6858.731.64
21573732-157373258.14459.53
31537123-153712356.79158.18
41564969-156496957.82059.12
51553150-155315057.38358.73
61508941-150894155.75057.12
60min11530156-153015656.53457.851.9458.2259.531.87
21592016-159201658.81960.53
31579771-157977158.36760.07
41596758-159675858.99460.62
51568883-156888357.96559.63
61527423-152742356.43358.12
极限11606093-160609359.33959.570.9261.3461.560.87
21623682-162368259.98962.02
31598905-159890559.07461.10
41627509-162750960.13162.08
51624051-162405160.00361.99
61593251-159325158.86560.86
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