布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.022675306269309826859802676797268136126825080.28
210.972692636269824226954390.15
单位质量响应值RSD%判断
243421.78245710.030.67数据可信
供试品溶液-250226083批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11163303-116330342.76841.821.6742.7741.821.68
21149056-114905642.24442.24
31114156-111415640.96140.96
41141217-114121741.95641.96
51140041-114004141.91241.91
61116690-111669041.05441.05
10min11315704-131570448.37048.221.0748.6148.451.06
21305802-130580248.00648.24
31318987-131898748.49148.72
41332759-133275948.99749.23
51303337-130333747.91648.15
61292823-129282347.52947.76
15min11343744-134374449.40150.091.4249.9150.591.41
21369152-136915250.33550.84
31383746-138374650.87251.37
41369224-136922450.33850.84
51374549-137454950.53451.03
61333820-133382049.03649.53
20min11352014-135201449.70548.592.0550.4949.372.03
21276593-127659346.93347.71
31319449-131944948.50849.29
41341825-134182549.33150.12
51332245-133224548.97949.76
61308154-130815448.09348.86
30min11268665-126866546.64145.167.6547.7046.217.48
21327592-132759248.80749.85
31084700-108470039.87840.93
41311946-131194648.23249.29
51157802-115780242.56543.62
61220057-122005744.85445.89
45min11406682-140668251.71548.0810.1453.0349.389.87
21394117-139411751.25352.57
31227155-122715545.11546.39
41174819-117481943.19144.52
51170057-117005743.01644.30
61473238-147323854.16255.44
60min11459331-145933153.65149.879.0455.2551.448.77
21454028-145402853.45655.05
31280723-128072347.08448.61
41236779-123677945.46947.04
51486349-148634954.64456.17
61221858-122185844.92046.50
极限11527870-152787056.17051.829.8158.0753.669.44
21178681-117868143.33345.23
31521616-152161655.94157.72
41410437-141043751.85353.67
51497714-149771455.06256.89
61321008-132100848.56550.40
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.022645331264621526449792643210263963626438740.10
210.972637782263791326378480.01
单位质量响应值RSD%判断
239915.97240460.160.17数据可信
供试品溶液-250226083批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11249111-124911146.75843.0410.1646.7643.0410.16
21258828-125882847.12247.12
31250359-125035946.80546.80
41100325-110032541.18941.19
51025715-102571538.39638.40
61013843-101384337.95137.95
10min11321919-132191949.48447.992.9249.7448.222.89
21244999-124499946.60446.87
31236963-123696346.30446.56
41324585-132458549.58349.81
51290735-129073548.31648.53
61272498-127249847.63447.84
15min11269929-126992947.53847.602.3148.0748.102.28
21217447-121744745.57346.09
31289492-128949248.27048.79
41302328-130232848.75049.25
51281730-128173047.97948.46
61268160-126816047.47147.95
20min11158416-115841643.36345.085.4144.1645.855.33
21180133-118013344.17644.95
31262803-126280347.27148.06
41269372-126937247.51748.29
51246246-124624646.65147.40
61109208-110920841.52142.26
30min11221815-122181545.73647.627.2846.7848.647.08
21164926-116492643.60744.63
31264891-126489147.34948.40
41254922-125492246.97648.01
51286172-128617248.14649.15
61440167-144016753.91054.88
45min11271615-127161547.60147.079.1548.8948.368.89
21181989-118198944.24645.51
31117516-111751641.83243.14
41274195-127419547.69749.00
51242085-124208546.49547.77
61457712-145771254.56755.84
60min11112497-111249741.64446.5510.2443.2048.099.93
21255210-125521046.98748.49
31161559-116155943.48145.02
41289973-128997348.28849.85
51174804-117480443.97745.51
61467185-146718554.92156.49
极限11432579-143257953.62651.187.4355.4252.987.15
21387796-138779651.95053.72
31374988-137498851.47053.26
41501514-150151456.20658.04
51288726-128872648.24150.02
61217020-121702045.55747.43
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