依折麦布阿托伐他汀片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DJ333-221017对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.67对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.221675771688651696661701731701891692940.66
210.161646751650981648860.19
单位质量响应值RSD%判断
16564.9716228.941.45数据可信
供试品溶液-2023121421批-依折麦布-pH6.8(内含0.2%Tween)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144057-4405724.10526.1215.0924.1026.1215.09
248437-4843726.50126.50
359644-5964432.63332.63
442054-4205423.00923.01
540390-4039022.09922.10
651892-5189228.39228.39
10min1116219-11621963.58767.807.2263.7267.947.23
2114460-11446062.62462.77
3138283-13828375.65975.84
4125864-12586468.86468.99
5119854-11985465.57665.70
6128837-12883770.49070.65
15min1154027-15402784.27385.382.2784.7685.902.28
2150500-15050082.34382.84
3158516-15851686.72987.33
4160613-16061387.87688.39
5156741-15674185.75786.24
6155889-15588985.29185.84
20min1166948-16694891.34291.511.7292.3092.501.74
2163233-16323389.30990.26
3169426-16942692.69893.78
4171249-17124993.69594.69
5165175-16517590.37291.34
6167477-16747791.63192.65
30min1171091-17109193.60995.281.6495.0796.781.64
2172529-17252994.39695.84
3174338-17433895.38596.98
4179372-17937298.14099.66
5173110-17311094.71396.18
6174420-17442095.43096.96
45min1174039-17403995.22296.821.7097.2098.851.70
2178220-17822097.50999.48
3177282-17728296.99699.12
4181337-18133799.215101.28
5173071-17307194.69296.68
6177798-17779897.27899.34
60min1173870-17387095.12995.621.1797.6498.191.18
2175041-17504195.77098.28
3177188-17718896.94599.61
4176943-17694396.81199.43
5173617-17361794.99197.51
6171926-17192694.06696.67
极限1173904-17390495.14895.522.0598.1998.621.98
2180745-18074598.891101.94
3173562-17356294.96198.17
4176415-17641596.52299.68
5170681-17068193.38496.43
6172199-17219994.21597.34
依折麦布阿托伐他汀片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100590-202005对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数2500
标示量(mg)20供试品稀释倍数5系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.143047193071713085703089813092623077410.61
211.073026523032763029640.15
单位质量响应值RSD%判断
27624.8727368.020.67数据可信
供试品溶液-2023121421批-阿托伐他汀-pH6.8(内含0.2%Tween)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1174749-17474952.49663.0429.3552.5063.0429.35
2249680-24968075.00675.01
3259889-25988978.07378.07
4104116-10411631.27731.28
5211178-21117863.44063.44
6259455-25945577.94377.94
10min1291500-29150087.56989.225.9087.8689.575.99
2306597-30659792.10592.52
3311690-31169093.63594.07
4263972-26397279.30079.47
5305146-30514691.66992.02
6303141-30314191.06691.50
15min1307709-30770992.43993.133.7393.2293.973.80
2325836-32583697.88498.81
3314655-31465594.52595.48
4292189-29218987.77688.39
5315788-31578894.86695.73
6303789-30378991.26192.20
20min1314120-31412094.36594.012.3795.6695.372.45
2322743-32274396.95598.43
3318433-31843395.66097.14
4301639-30163990.61591.72
5311756-31175693.65495.04
6308935-30893592.80794.25
30min1310879-31087993.39194.561.1195.2196.441.17
2319389-31938995.94797.96
3317835-31783595.48197.49
4314068-31406894.34995.95
5315435-31543594.76096.67
6311001-31100193.42895.39
45min1314137-31413794.37095.131.2996.7097.541.31
2323415-32341597.15799.70
3318888-31888895.79798.34
4317273-31727395.31297.44
5312657-31265793.92596.36
6313662-31366294.22796.71
60min1312832-31283293.97893.851.7196.8496.791.71
2315961-31596194.91898.00
3318383-31838395.64598.72
4310658-31065893.32495.98
5313586-31358694.20497.16
6303008-30300891.02694.03
极限1312821-31282193.97493.752.3597.3697.212.33
2325577-32557797.806101.42
3311431-31143193.55797.16
4310464-31046493.26696.44
5308332-30833292.62696.11
6303825-30382591.27294.78
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢鑫慧 于 2024-04-19 15:10:30 完成)
生成报告数据部分(等待生成报告)
Current page cost:60 ms