阿齐沙坦片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号68522100802对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.70对照品水分(%)0对照品稀释倍数1000
标示量(mg)20供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.222955212960102962952956942927592952560.49
211.122956402957912957160.04
单位质量响应值RSD%判断
26315.1526593.170.75数据可信
供试品溶液-25112801批-pH5.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min117500-175005.9368.2215.575.948.2215.57
228621-286219.7089.71
325895-258958.7848.78
425636-256368.6968.70
524764-247648.4008.40
622979-229797.7947.79
10min163149-6314921.42030.0116.4621.4530.0616.46
293855-9385531.83631.89
3102745-10274534.85134.90
499762-9976233.83933.89
581057-8105727.49527.54
690322-9032230.63730.68
15min1105474-10547435.77746.0311.3235.9346.2411.33
2140671-14067147.71647.95
3146573-14657349.71849.96
4144751-14475149.10049.34
5134748-13474845.70745.91
6141908-14190848.13548.35
20min1145390-14539049.31656.716.5049.6757.186.55
2172061-17206158.36358.86
3173745-17374558.93459.45
4172445-17244558.49359.00
5167884-16788456.94657.40
6171590-17159058.20358.68
30min1193411-19341165.60568.392.0266.2369.172.11
2202722-20272268.76369.58
3202583-20258368.71669.56
4203166-20316668.91469.75
5204285-20428569.29370.06
6203548-20354869.04369.85
45min1226504-22650476.83077.680.8877.8278.850.93
2229739-22973977.92779.13
3228928-22892877.65278.88
4227438-22743877.14778.36
5229218-22921877.75178.91
6232302-23230278.79779.98
60min1245675-24567583.33383.110.9984.7584.700.95
2246099-24609983.47785.11
3244923-24492383.07884.74
4240256-24025681.49583.14
5246609-24660983.65085.24
6246516-24651683.61885.24
极限1257149-25714987.22587.520.3389.1089.580.38
2258608-25860887.72089.82
3258354-25835487.63489.75
4256844-25684487.12189.22
5258965-25896587.84189.89
6258213-25821387.58689.68
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