贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.223042123012213011463012103011343017850.45
210.153026863024663025760.06
单位质量响应值RSD%判断
29528.8629810.440.68数据可信
供试品溶液-24041801SP批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1146728-14672849.31752.093.7949.3252.093.79
2149755-14975550.33450.33
3155400-15540052.23152.23
4159170-15917053.49853.50
5156231-15623152.51152.51
6162568-16256854.64054.64
10min1224628-22462875.49977.211.1575.5877.291.15
2229877-22987777.26477.35
3229908-22990877.27477.36
4230679-23067977.53377.62
5230930-23093077.61877.71
6232202-23220278.04578.14
15min1249537-24953783.87285.070.9884.0885.280.98
2251973-25197384.69084.90
3252660-25266084.92185.14
4253415-25341585.17585.39
5253956-25395685.35785.57
6257012-25701286.38486.61
20min1260255-26025587.47488.760.8587.8289.120.86
2263499-26349988.56488.92
3263944-26394488.71489.07
4264507-26450788.90389.26
5265221-26522189.14389.50
6267027-26702789.75090.12
30min1273003-27300391.75993.170.9792.2593.670.98
2276308-27630892.86993.37
3277485-27748593.26593.77
4277149-27714993.15293.66
5277855-27785593.38993.90
6281345-28134594.56295.08
45min1283660-28366095.34196.640.7995.9997.300.79
2287748-28774896.71597.37
3287525-28752596.64097.30
4287391-28739196.59597.26
5288114-28811496.83897.50
6290661-29066197.69498.37
60min1288476-28847696.95998.120.7297.7698.940.73
2290976-29097697.80098.62
3292396-29239698.27799.10
4292545-29254598.32799.15
5292447-29244798.29499.12
6294764-29476499.07399.91
极限1291440-29144097.95599.200.7898.92100.180.79
2294827-29482799.094100.07
3296030-29603099.498100.48
4294576-29457699.010100.00
5295499-29549999.320100.31
6298500-298500100.328101.33
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