熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号U202302006对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.223677736643369193676136750367700.27
211.123679836703367500.19
单位质量响应值RSD%判断
3277.183304.860.60数据可信
供试品溶液-25112801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127451-2745174.77274.723.6474.7774.723.64
227674-2767475.37975.38
327520-2752074.96074.96
425637-2563769.83169.83
527601-2760175.18075.18
628719-2871978.22578.23
10min133487-3348791.21391.461.2491.3491.591.24
233791-3379192.04192.17
333588-3358891.48891.61
432827-3282789.41589.53
534042-3404292.72492.85
633741-3374191.90592.03
15min134736-3473694.61594.370.9994.8994.640.99
234053-3405392.75493.03
334941-3494195.17395.45
434493-3449393.95394.22
534981-3498195.28295.56
634667-3466794.42794.71
20min136092-3609298.30896.051.3798.7496.481.36
235336-3533696.24996.68
335131-3513195.69196.13
434922-3492295.12195.54
535384-3538496.38096.82
634704-3470494.52894.97
30min134280-3428093.37395.421.6093.9796.021.59
235980-3598098.00398.60
334841-3484194.90195.50
435044-3504495.45496.03
535188-3518895.84696.45
634855-3485594.93995.54
45min134843-3484394.90695.540.7595.6696.300.75
235358-3535896.30997.07
335167-3516795.78996.54
435120-3512095.66196.40
535289-3528996.12196.88
634684-3468494.47395.23
60min136028-3602898.13496.001.3799.0596.921.36
235343-3534396.26897.19
334552-3455294.11495.03
435286-3528696.11397.01
535266-3526696.05896.98
635002-3500295.33996.25
极限135003-3500395.34295.670.6596.4296.740.65
235318-3531896.20097.28
335146-3514695.73296.80
434817-3481794.83595.89
535440-3544096.53297.61
635017-3501795.38096.45
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号U202302006对照品来源自制对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.223691436692368553690036963368650.29
211.123720537096371500.21
单位质量响应值RSD%判断
3285.653340.831.18数据可信
供试品溶液-25121001批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min128773-2877377.85174.005.3577.8574.005.34
224818-2481867.15067.15
328674-2867477.58377.58
427756-2775675.09975.10
526792-2679272.49172.49
627295-2729573.85273.85
10min133794-3379491.43689.332.0091.5789.462.00
231964-3196486.48586.60
333528-3352890.71790.85
432977-3297789.22689.35
532629-3262988.28488.41
633207-3320789.84889.97
15min134870-3487094.34893.520.9094.6393.800.90
234087-3408792.22992.49
334673-3467393.81594.10
434322-3432292.86593.14
534588-3458893.58593.85
634851-3485194.29694.57
20min134977-3497794.63794.630.5495.0895.060.54
235054-3505494.84695.26
335143-3514395.08695.52
434774-3477494.08894.52
534729-3472993.96694.39
635171-3517195.16295.59
30min135638-3563896.42695.251.2897.0295.831.27
234908-3490894.45095.02
335642-3564296.43697.03
434594-3459493.60194.19
534935-3493594.52495.10
635501-3550196.05596.64
45min135333-3533395.60094.621.0296.3695.371.02
235068-3506894.88395.61
334989-3498994.67095.43
434317-3431792.85193.59
534909-3490994.45395.19
635216-3521695.28496.03
60min135026-3502694.77094.641.0495.6995.541.04
234945-3494594.55195.43
334625-3462593.68594.60
434656-3465693.76994.66
534984-3498494.65695.55
635632-3563296.40997.32
极限135301-3530195.51494.881.0796.5995.941.06
235645-3564596.44597.49
334942-3494294.54295.61
434596-3459693.60694.66
534807-3480794.17795.23
635100-3510094.97096.04
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