熊取样颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号U202302006对照品来源自制对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.013592135879358283547135385356970.70
210.993542535719355720.59
单位质量响应值RSD%判断
3242.233236.760.12数据可信
供试品溶液-5122401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min128324-2832478.61172.088.7078.6172.098.69
222024-2202461.12661.13
326065-2606572.34272.34
425902-2590271.88971.89
528005-2800577.72677.73
625515-2551570.81570.82
10min134551-3455195.89491.033.9596.0291.153.95
230768-3076885.39585.50
333734-3373493.62693.75
432493-3249390.18290.30
532881-3288191.25991.39
632367-3236789.83289.95
15min136063-36063100.09097.721.82100.3897.991.83
234174-3417494.84895.09
335633-3563398.89799.17
435293-3529397.95398.22
534997-3499797.13297.41
635098-3509897.41297.68
20min136282-36282100.69899.541.00101.1699.971.01
235419-3541998.30398.71
336175-36175100.401100.84
436067-36067100.102100.53
535554-3555498.67899.12
635689-3568999.05299.48
30min136301-36301100.75199.800.84101.38100.400.85
235745-3574599.20899.77
335962-3596299.810100.42
436297-36297100.740101.34
535539-3553998.63699.24
635916-3591699.682100.28
45min136117-36117100.24099.680.50101.03100.440.50
235914-3591499.677100.41
335917-3591799.685100.46
436099-36099100.190100.96
535663-3566398.98099.75
635774-3577499.288100.05
60min135990-3599099.88899.400.62100.85100.340.63
235602-3560298.81199.71
336051-36051100.057101.00
435962-3596299.810100.75
535519-3551998.58199.52
635766-3576699.266100.19
极限136115-36115100.23599.300.54101.36100.400.55
235702-3570299.088100.15
335815-3581599.402100.51
435823-3582399.424100.53
535557-3555798.68699.79
635660-3566098.972100.06
熊取样颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号U202302006对照品来源自制对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.013555335644357643599935877357670.50
210.993571435861357880.30
单位质量响应值RSD%判断
3248.593256.410.18数据可信
供试品溶液-5122402批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126966-2696674.54377.202.9474.5477.202.95
228309-2830978.25678.26
328014-2801477.44077.44
427788-2778876.81576.82
529261-2926180.88780.89
627225-2722575.25975.26
10min133887-3388793.67593.621.3793.8093.751.37
234074-3407494.19294.32
333958-3395893.87194.00
433390-3339092.30192.43
534573-3457395.57195.71
633326-3332692.12492.25
15min135432-3543297.94697.351.0298.2397.641.02
235335-3533597.67897.97
335432-3543297.94698.23
434866-3486696.38196.66
535560-3556098.30098.59
634675-3467595.85396.13
20min135958-3595899.40098.031.4199.8498.481.41
235719-3571998.73999.19
335748-3574898.81999.27
434600-3460095.64696.09
535588-3558898.37798.84
635167-3516797.21397.65
30min135993-3599399.49798.961.80100.1199.571.80
236533-36533100.989101.60
335864-3586499.14099.75
434824-3482496.26596.87
536303-36303100.354100.98
635266-3526697.48798.09
45min136408-36408100.64498.942.00101.4299.722.00
236538-36538101.003101.79
335948-3594899.372100.15
434771-3477196.11996.88
536012-3601299.549100.34
635079-3507996.97097.73
60min136104-3610499.80498.451.30100.7599.391.30
235632-3563298.49999.45
335860-3586099.129100.07
435000-3500096.75297.67
535980-3598099.461100.42
635112-3511297.06197.99
极限135980-3598099.46198.371.26100.5799.481.26
235762-3576298.85899.97
335555-3555598.28699.40
434983-3498396.70597.79
536089-3608999.762100.88
635148-3514897.16198.25
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