苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.159065890755907429066890715907080.05
214.169073090831907800.08
单位质量响应值RSD%判断
6410.466411.020.01数据可信
供试品溶液-2024031812批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min189286-8928697.72098.410.9597.7298.410.95
290429-9042998.97198.97
391331-9133199.95899.96
489333-8933397.77197.77
589975-8997598.47498.47
689138-8913897.55897.56
10min188050-8805096.36797.261.3197.3498.251.30
288865-8886597.25998.25
389481-8948197.93398.93
487388-8738895.64396.62
588709-8870997.08998.07
690724-9072499.294100.27
15min189330-8933097.76897.980.5899.7199.940.57
289379-8937997.82299.78
390137-9013798.651100.63
489983-8998398.483100.42
588717-8871797.09799.05
689617-8961798.082100.05
20min186548-8654894.72396.481.4597.6499.421.42
289574-8957498.035100.98
389778-8977898.259101.22
487550-8755095.82098.74
588061-8806196.37999.31
687432-8743295.69198.64
30min186311-8631194.46495.421.2298.3399.321.17
285769-8576993.87197.79
387074-8707495.29999.25
487640-8764095.91999.80
587535-8753595.80499.69
688757-8875797.141101.05
45min185979-8597994.10194.860.6798.9199.720.66
286186-8618694.32799.19
386643-8664394.82799.73
486550-8655094.72699.56
587191-8719195.427100.28
687497-8749795.762100.64
60min182215-8221589.98193.292.5895.7399.102.46
286794-8679494.993100.80
386123-8612394.258100.11
482648-8264890.45596.24
586730-8673094.923100.73
686935-8693595.147100.98
极限181790-8179089.51692.151.5496.1798.891.47
284446-8444692.42399.18
385345-8534593.407100.20
485054-8505493.08899.78
584753-8475392.75999.51
683810-8381091.72798.51
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