苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.159022290199903879048190478903530.16
214.168980089828898140.03
单位质量响应值RSD%判断
6385.376342.800.48数据可信
供试品溶液-2024031811批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min185655-8565594.43494.442.2294.4394.442.23
282180-8218090.60390.60
386286-8628695.13095.13
485379-8537994.13094.13
587728-8772896.72096.72
686754-8675495.64695.65
10min185944-8594494.75392.912.1895.7093.852.17
282080-8208090.49391.40
382140-8214090.55991.51
485197-8519793.92994.87
586201-8620195.03696.00
684054-8405492.66993.63
15min187657-8765796.64296.131.6798.5398.001.67
284271-8427192.90994.72
387688-8768896.67698.53
488054-8805497.07998.96
587443-8744396.40698.32
688049-8804997.07498.96
20min186383-8638395.23795.161.3698.1097.991.35
285670-8567094.45197.19
384392-8439293.04295.87
486644-8664495.52598.38
587790-8779096.78899.67
686981-8698195.89698.75
30min184670-8467093.34892.911.0697.1696.701.01
285231-8523193.96797.65
383521-8352192.08295.84
483969-8396992.57696.38
585172-8517293.90297.75
683087-8308791.60395.42
45min185094-8509493.81693.131.5698.5697.851.50
283032-8303291.54396.17
383800-8380092.38997.06
485185-8518593.91698.65
583304-8330491.84296.63
686421-8642195.279100.01
60min180402-8040288.64391.882.1694.3397.522.01
284197-8419792.82798.37
383254-8325491.78797.39
484138-8413892.76298.43
582410-8241090.85796.56
685616-8561694.391100.07
极限183449-8344992.00291.362.0498.5797.931.96
279830-7983088.01294.48
382369-8236990.81297.33
482973-8297391.47798.08
584683-8468393.36399.98
683904-8390492.50499.13
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.159080090611909589102691069908930.21
214.169110291239911700.11
单位质量响应值RSD%判断
6423.536438.560.17数据可信
供试品溶液-2024031811批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min185578-8557893.36693.532.1693.3793.532.16
285231-8523192.98892.99
388831-8883196.91596.92
485742-8574293.54593.55
585924-8592493.74493.74
683069-8306990.62990.63
10min184377-8437792.05692.661.9992.9993.601.98
285550-8555093.33694.27
386334-8633494.19195.16
487119-8711995.04795.98
582879-8287990.42291.36
683340-8334090.92491.83
15min188466-8846696.51795.391.7298.3797.251.71
288139-8813996.16098.02
387577-8757795.54797.46
488248-8824896.27998.17
587708-8770895.69097.53
684439-8443992.12393.94
20min187029-8702994.94994.081.3497.7796.891.34
286462-8646294.33197.16
387734-8773495.71898.58
486232-8623294.08096.93
584476-8447692.16494.96
685439-8543993.21495.95
30min182239-8223989.72392.331.4793.4996.081.41
285449-8544993.22596.99
385026-8502692.76496.59
485181-8518192.93396.72
584330-8433092.00595.72
685522-8552293.30596.97
45min186766-8676694.66292.441.4799.3397.121.41
285021-8502192.75897.46
383822-8382291.45096.20
485416-8541693.18997.91
583751-8375191.37396.01
683617-8361791.22795.83
60min185995-8599593.82191.062.5699.4396.662.39
284418-8441892.10197.73
382948-8294890.49796.16
479666-7966686.91692.57
583440-8344091.03496.59
684296-8429691.96797.48
极限183707-8370791.32590.292.0297.8896.801.93
282364-8236489.86096.41
384489-8448992.17898.75
483503-8350391.10297.62
582751-8275190.28296.75
679711-7971186.96593.40
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.159267092657925279261892599926140.07
214.169190392021919620.10
单位质量响应值RSD%判断
6545.166494.490.55数据可信
供试品溶液-2024031812批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min186812-8681293.42495.131.8993.4295.131.89
290135-9013597.00097.00
388333-8833395.06195.06
490558-9055897.45597.46
588027-8802794.73294.73
686513-8651393.10293.10
10min186304-8630492.87796.732.5393.8197.682.52
292592-9259299.644100.61
388883-8888395.65396.60
491590-9159098.56699.54
590892-9089297.81598.76
689066-8906695.85096.78
15min187583-8758394.25494.571.2996.1296.491.28
289779-8977996.61798.58
388035-8803594.74096.65
487543-8754394.21196.17
586294-8629492.86794.79
688047-8804794.75396.64
20min186016-8601692.56793.461.1695.3796.321.14
287570-8757094.24097.17
387765-8776594.45097.30
487121-8712193.75796.66
585235-8523591.72794.58
687354-8735494.00796.84
30min185276-8527691.77192.901.5795.5096.701.55
287484-8748494.14798.02
386478-8647893.06596.86
488082-8808294.79198.63
584437-8443790.86894.64
686176-8617692.74096.52
45min182366-8236688.63990.722.1393.2995.452.09
286865-8686593.48198.30
384575-8457591.01795.75
485716-8571692.24597.03
582446-8244688.72693.41
683831-8383190.21694.92
60min184145-8414590.55491.031.3296.0996.661.31
286781-8678193.39199.14
383722-8372290.09995.74
484529-8452990.96796.68
583951-8395190.34595.91
684374-8437490.80096.41
极限180789-8078986.94289.441.5293.3895.981.47
283956-8395690.35197.04
382901-8290189.21595.76
483568-8356889.93396.55
584342-8434290.76697.24
683079-8307989.40795.92
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