苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.158943789891898528951889700896800.23
214.169004690151900980.09
单位质量响应值RSD%判断
6337.816362.850.28数据可信
供试品溶液-2024031813批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min187554-8755496.73695.661.8396.7495.661.83
287836-8783697.04897.05
387284-8728496.43896.44
486600-8660095.68295.68
586701-8670195.79495.79
683504-8350492.26292.26
10min188909-8890998.23397.022.7799.2097.972.73
288558-8855897.84698.82
383693-8369392.47093.43
486292-8629295.34296.30
588911-8891198.23699.19
690482-9048299.971100.89
15min187351-8735196.51297.660.8898.4699.580.86
288377-8837797.64699.59
389011-8901198.346100.24
487559-8755996.74298.65
588787-8878798.099100.04
689229-8922998.587100.51
20min186904-8690496.01896.752.2798.9399.652.21
287249-8724996.39999.32
384488-8448893.34996.22
489890-8989099.317102.19
587251-8725196.40299.32
689604-8960499.001101.91
30min189025-8902598.36296.921.30102.24100.791.26
287186-8718696.330100.22
386048-8604895.07298.88
488643-8864397.940101.81
588336-8833697.600101.49
687086-8708696.219100.12
45min188907-8890798.23197.541.49103.09102.381.42
288411-8841197.683102.54
388466-8846697.744102.50
486518-8651895.592100.44
587145-8714596.284101.15
690230-9023099.693104.55
60min185930-8593094.94296.731.07100.78102.540.99
287734-8773496.935102.76
388652-8865297.949103.68
487518-8751896.697102.50
587293-8729396.448102.27
688170-8817097.417103.27
极限183886-8388692.68494.621.5099.47101.401.42
285324-8532494.272101.07
385409-8540994.366101.08
486326-8632695.380102.15
585156-8515694.087100.88
687716-8771696.915103.75
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.158955189502900339004389714897690.29
214.169115991200911800.04
单位质量响应值RSD%判断
6344.106439.271.06数据可信
供试品溶液-2024031813批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min179702-7970287.49688.622.6387.5088.622.63
279534-7953487.31187.31
378931-7893186.64986.65
481182-8118289.12089.12
580214-8021488.05888.06
684770-8477093.05993.06
10min184965-8496593.27392.811.0694.1593.691.02
284812-8481293.10593.98
385332-8533293.67694.54
485031-8503193.34694.24
584200-8420092.43393.31
682895-8289591.00191.93
15min184955-8495593.26295.261.8095.0797.071.77
286157-8615794.58296.39
389164-8916497.88399.69
487987-8798796.59198.42
586728-8672895.20997.01
685648-8564894.02395.86
20min185830-8583094.22393.970.8496.9696.740.81
285105-8510593.42796.18
384793-8479393.08495.87
486742-8674295.22498.01
585960-8596094.36697.12
685185-8518593.51596.30
30min184922-8492293.22692.050.8496.9195.760.79
283887-8388792.09095.77
383027-8302791.14694.86
483235-8323591.37495.12
583730-8373091.91895.62
684318-8431892.56396.28
45min180572-8057288.45191.552.4693.0796.182.34
284732-8473293.01897.62
386231-8623194.66399.29
484090-8409092.31396.97
582938-8293891.04895.67
681825-8182589.82694.47
60min184162-8416292.39292.290.6297.8997.840.58
284588-8458892.85998.39
384538-8453892.80598.38
483619-8361991.79697.38
583300-8330091.44596.98
684224-8422492.46098.00
极限181679-8167989.66690.420.5196.0996.880.48
282630-8263090.71097.17
382150-8215090.18396.68
482357-8235790.41096.91
582487-8248790.55397.00
682866-8286690.96997.43
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.159035190469903649026190732904350.21
214.169069490263904780.34
单位质量响应值RSD%判断
6391.176389.690.02数据可信
供试品溶液-2024032611批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min185777-8577794.17894.651.6194.1894.651.61
288613-8861397.29297.29
385850-8585094.25894.26
486506-8650694.97894.98
586127-8612794.56294.56
684364-8436492.62792.63
10min186410-8641094.87393.930.8295.8194.870.81
285773-8577394.17495.15
384776-8477693.07994.02
485063-8506393.39494.34
585013-8501393.33994.28
686262-8626294.71095.64
15min183518-8351891.69893.361.2893.5995.241.25
284838-8483893.14795.06
384093-8409392.32994.20
485680-8568094.07195.96
586368-8636894.82796.71
685689-8568994.08195.95
20min183635-8363591.82691.420.6394.6394.240.60
282457-8245790.53393.38
383132-8313291.27494.07
483050-8305091.18494.01
583369-8336991.53494.36
683958-8395892.18194.99
30min184206-8420692.45391.731.3796.1895.471.33
284001-8400192.22895.98
381560-8156089.54893.26
483111-8311191.25194.99
584855-8485593.16696.91
683570-8357091.75595.49
45min183235-8323591.38790.172.2296.0494.822.11
283387-8338791.55496.23
383189-8318991.33695.94
482841-8284190.95495.60
581396-8139689.36894.04
678721-7872186.43191.08
60min180903-8090388.82789.211.4794.3994.761.40
282814-8281490.92596.51
382052-8205290.08895.61
481400-8140089.37294.93
581041-8104188.97894.55
679305-7930587.07292.59
极限181214-8121489.16889.820.7495.6296.260.70
281580-8158089.57096.07
381211-8121189.16595.58
482192-8219290.24296.69
582760-8276090.86597.32
681897-8189789.91896.31
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.158958089593895208967089802896330.13
214.169066990799907340.11
单位质量响应值RSD%判断
6334.496407.770.82数据可信
供试品溶液-2024032611批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min185750-8575094.43795.561.1594.4495.561.15
286281-8628195.02195.02
385994-8599494.70594.71
486673-8667395.45395.45
587638-8763896.51696.52
688281-8828197.22497.22
10min186320-8632095.06494.410.7596.0195.370.74
286590-8659095.36296.31
385532-8553294.19795.14
485259-8525993.89694.85
584895-8489593.49594.46
685769-8576994.45895.43
15min183572-8357292.03893.781.6493.9395.681.61
284621-8462193.19395.10
384463-8446393.01994.91
485442-8544294.09795.99
587676-8767696.55898.46
685123-8512393.74695.66
20min183559-8355992.02491.501.3494.8494.341.31
281118-8111889.33592.17
383146-8314691.56994.39
483443-8344391.89694.73
584452-8445293.00795.87
682791-8279191.17894.03
30min184523-8452393.08592.141.2696.8295.891.22
283958-8395892.46396.19
381819-8181990.10793.84
483047-8304791.46095.21
584434-8443492.98796.78
684223-8422392.75596.52
45min182826-8282691.21690.802.0195.8895.481.92
279135-7913587.15291.81
383054-8305491.46896.10
482966-8296691.37196.04
583021-8302191.43196.16
683703-8370392.18296.88
60min181233-8123389.46290.110.7895.0495.690.74
281407-8140789.65495.18
382263-8226390.59696.15
481878-8187890.17295.75
581308-8130889.54595.18
682832-8283291.22396.84
极限181228-8122889.45790.330.6695.9396.820.63
282426-8242690.77697.20
381996-8199690.30296.76
481804-8180490.09196.57
582786-8278691.17297.71
681898-8189890.19496.72
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