布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.472760967276114127622682762800276377327621900.05
211.352758296275986527590800.05
单位质量响应值RSD%判断
240818.66243090.750.67数据可信
冻融3天-供试品溶液-2025110251批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12557922-255792295.05494.060.7495.0594.060.74
22547305-254730594.66094.66
32531310-253131094.06594.07
42508762-250876293.22793.23
52516812-251681293.52693.53
62524615-252461593.81693.82
10min12570043-257004395.50594.000.9896.0394.520.98
22535618-253561894.22594.75
32520267-252026793.65594.18
42496468-249646892.77093.29
52518201-251820193.57894.10
62537132-253713294.28294.80
15min12558310-255831095.06993.940.9596.1394.990.95
22538508-253850894.33395.38
32525961-252596193.86694.91
42489486-248948692.51193.54
52515311-251531193.47194.51
62540836-254083694.41995.46
20min12537881-253788194.30993.450.9695.9095.010.96
22527573-252757393.92695.50
32514910-251491093.45695.02
42471933-247193391.85993.41
52504961-250496193.08694.64
62530777-253077794.04595.61
30min12537753-253775394.30593.141.2096.4295.221.20
22526360-252636093.88195.98
32507038-250703893.16395.25
42454268-245426891.20293.26
52492311-249231192.61694.69
62520472-252047293.66295.75
极限12514219-251421993.43092.681.0196.0695.281.01
22496512-249651292.77295.39
32496284-249628492.76495.36
42445765-244576590.88693.45
52497951-249795192.82695.42
62513819-251381993.41596.03
布洛芬混悬液项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100179-202308对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数50
标示量(mg)200供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.472763774276212227612572762425275881927616790.07
211.352764194275873127614620.14
单位质量响应值RSD%判断
240774.11243300.620.74数据可信
冻融3天-供试品溶液-250226083批-pH7.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12536854-253685494.23994.490.5094.2494.490.50
22539923-253992394.35394.35
32540625-254062594.38094.38
42568688-256868895.42295.42
52540483-254048394.37494.37
62535046-253504694.17294.17
10min12576341-257634195.70696.372.4296.2396.892.41
22570597-257059795.49396.02
32569004-256900495.43495.96
42577586-257758695.75396.28
52720675-2720675101.068101.59
62550491-255049194.74695.27
15min12579591-257959195.82795.400.3996.8896.460.38
22571164-257116495.51496.57
32573811-257381195.61296.67
42571973-257197395.54496.61
52556368-255636894.96496.05
62555448-255544894.93095.98
20min12571160-257116095.51496.613.8397.1098.203.76
22564132-256413295.25396.84
32802721-2802721104.116105.70
42565387-256538795.29996.89
52555082-255508294.91796.53
62545115-254511594.54696.12
30min12554310-255431094.88894.790.3497.0196.920.35
22553954-255395494.87596.99
32561210-256121095.14497.31
42556645-255664594.97597.10
52546428-254642894.59596.74
62536987-253698794.24496.35
极限12537829-253782994.27694.380.3996.9297.040.40
22541209-254120994.40197.04
32555008-255500894.91497.61
42546261-254626194.58997.24
52538672-253867294.30796.97
62525526-252552693.81996.44
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