枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.489521909529139511749531079528119524390.09
217.399521289540739531000.15
单位质量响应值RSD%判断
54487.3654807.360.42数据可信
影响因素30天高温-供试品溶液-8167339批-100mg规格-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11048253-104825397.12991.329.4097.1391.329.40
21023348-102334894.82194.82
31028090-102809095.26195.26
4995413-99541392.23392.23
5799825-79982574.11074.11
61018712-101871294.39294.39
10min11067321-106732198.89698.040.9099.0698.190.90
21058203-105820398.05198.21
31067483-106748398.91199.07
41056911-105691197.93198.08
51057090-105709097.94898.07
61041508-104150896.50496.66
15min11070524-107052499.19298.511.1099.5298.821.10
21063057-106305798.50198.82
31074377-107437799.54999.87
41060080-106008098.22598.54
51069171-106917199.06799.35
61041768-104176896.52896.85
20min11072772-107277299.40198.671.1599.8999.151.15
21068424-106842498.99899.48
31077918-107791899.878100.37
41059749-105974998.19498.67
51067013-106701398.86799.32
61043336-104333696.67397.15
30min11074148-107414899.52898.881.22100.1999.531.21
21067051-106705198.87199.52
31085027-1085027100.536101.19
41060407-106040798.25598.90
51069689-106968999.11599.73
61046720-104672096.98797.63
45min11078820-107882099.96198.961.27100.7899.771.27
21068020-106802098.96099.78
31082710-1082710100.322101.15
41058366-105836698.06698.87
51073538-107353899.472100.25
61046550-104655096.97197.77
极限11079502-1079502100.02498.871.20101.0199.851.19
21063466-106346698.53899.52
31080179-1080179100.087101.08
41058312-105831298.06199.03
51072992-107299299.421100.37
61048069-104806997.11298.08
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.489528529535299524329560619535599536870.15
217.399534299524099529190.08
单位质量响应值RSD%判断
54558.7554796.950.31数据可信
影响因素30天高湿-供试品溶液-8167339批-100mg规格-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11035349-103534995.87995.180.6195.8895.180.61
21031018-103101895.47895.48
31021694-102169494.61594.61
41019125-101912594.37794.38
51028203-102820395.21895.22
61031343-103134395.50895.51
10min11052599-105259997.47796.601.1197.6496.761.11
21049685-104968597.20797.37
31031305-103130595.50595.66
41048004-104800497.05197.21
51025850-102585095.00095.16
61051300-105130097.35697.52
15min11055034-105503497.70296.531.2398.0296.851.22
21045774-104577496.84597.17
31036503-103650395.98696.30
41051152-105115297.34397.66
51019705-101970594.43194.75
61046052-104605296.87097.19
20min11059130-105913098.08296.411.4798.5796.891.47
21040951-104095196.39896.88
31036043-103604395.94496.42
41049941-104994197.23197.71
51014506-101450693.94994.42
61046035-104603596.86997.35
30min11061440-106144098.29596.391.5498.9497.031.53
21041295-104129596.43097.07
31037706-103770696.09896.73
41050377-105037797.27197.91
51013545-101354593.86094.49
61040989-104098996.40297.05
45min11060771-106077198.23496.791.6299.0597.591.62
21039451-103945196.25997.06
31052862-105286297.50198.30
41055307-105530797.72898.53
51013880-101388093.89194.68
61048886-104888697.13397.94
极限11065086-106508698.63398.070.9399.6199.030.92
21044632-104463296.73997.70
31055607-105560797.75598.71
41071490-107149099.226100.19
51052936-105293697.50898.45
61064252-106425298.55699.52
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.489523709545769577289506349528679536350.29
217.399519709513199516440.05
单位质量响应值RSD%判断
54555.7854723.630.22数据可信
影响因素30天光照-供试品溶液-8167339批-100mg规格-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11035105-103510595.92394.732.3095.9294.742.30
21027570-102757095.22595.23
3990577-99057791.79791.80
41024711-102471194.96094.96
51055108-105510897.77797.78
61000605-100060592.72692.73
10min11059335-105933598.16997.511.8298.3397.671.82
21048162-104816297.13397.29
31034309-103430995.85096.00
41065564-106556498.74698.90
51078108-107810899.908100.07
61028028-102802895.26895.42
15min11069827-106982799.14197.691.6799.4698.011.67
21052421-105242197.52897.85
31042297-104229796.59096.90
41062031-106203198.41998.74
51071956-107195699.33899.67
61026286-102628695.10695.42
20min11069594-106959499.11997.601.6799.6198.081.68
21050545-105054597.35497.84
31043464-104346496.69897.17
41063564-106356498.56199.05
51068021-106802198.97499.47
61024077-102407794.90195.37
30min11073863-107386399.51597.621.62100.1798.261.61
21051114-105111497.40798.05
31046208-104620896.95297.59
41059749-105974998.20798.86
51064234-106423498.62399.28
61025032-102503294.99095.62
45min11073937-107393799.52297.781.58100.3498.591.58
21053604-105360497.63898.45
31046086-104608696.94197.74
41064320-106432098.63199.45
51065416-106541698.73299.56
61027627-102762795.23096.02
极限11070607-107060799.213100.406.31100.20101.376.26
21064804-106480498.67699.65
31045976-104597696.93197.89
41217962-1217962112.869113.85
51074468-107446899.571100.56
61026364-102636495.11396.06
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2026-01-14 16:48:04 完成)
生成报告数据部分下载报告(谢超君 于 2026-01-14 16:48:25 完成)
Current page cost:80 ms