替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.912614126205261972601526153261420.30
213.962621526307262610.25
单位质量响应值RSD%判断
1879.371881.160.07数据可信
供试品溶液-1批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111694-1169443.63148.656.5943.6348.656.59
212624-1262447.10147.10
313344-1334449.78749.79
413242-1324249.40649.41
514294-1429453.33153.33
613040-1304048.65348.65
10min116731-1673162.42468.597.8662.8669.077.83
218539-1853969.17069.64
316495-1649561.54362.04
419109-1910971.29671.79
519570-1957073.01673.55
619854-1985474.07674.56
15min120058-2005874.83778.432.7475.9079.602.77
220873-2087377.87879.04
321146-2114678.89680.01
420856-2085677.81479.02
521563-2156380.45281.72
621623-2162380.67681.90
20min119709-1970973.53579.014.4575.3480.974.45
220628-2062876.96478.91
320923-2092378.06479.97
421814-2181481.38983.37
522273-2227383.10185.17
621719-2171981.03483.07
30min121036-2103678.48680.392.5081.0383.132.56
221150-2115078.91181.62
321026-2102678.44981.13
421828-2182881.44184.24
522237-2223782.96785.87
621993-2199382.05784.90
45min119637-1963773.26677.713.6676.6081.263.66
220263-2026375.60279.10
320835-2083577.73681.20
421662-2166280.82284.44
521444-2144480.00883.74
621121-2112178.80382.47
60min117802-1780266.42074.836.3870.4879.166.21
219365-1936572.25276.51
320955-2095578.18482.43
420236-2023675.50179.92
521109-2110978.75883.29
620875-2087577.88582.34
极限120250-2025075.55374.952.2580.2880.032.18
219918-1991874.31579.29
319764-1976473.74078.77
419939-1993974.39379.57
520929-2092978.08783.40
619732-1973273.62178.85
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.912608526118260362619626121261110.23
213.962637026253263120.32
单位质量响应值RSD%判断
1877.141884.810.29数据可信
供试品溶液-2批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min112370-1237046.13642.939.9146.1442.939.92
211345-1134542.31342.31
310436-1043638.92238.92
410833-1083340.40340.40
510703-1070339.91839.92
613374-1337449.88049.88
10min117140-1714063.92666.245.9364.3966.675.87
216822-1682262.74063.16
317647-1764765.81766.21
417808-1780866.41766.82
519785-1978573.79174.19
617357-1735764.73565.23
15min120504-2050476.47279.062.3877.5780.152.39
220869-2086977.83478.88
321072-2107278.59179.64
421199-2119979.06580.13
521813-2181381.35582.49
621734-2173481.06082.21
20min120785-2078577.52177.894.1179.3979.774.05
219269-1926971.86673.70
321392-2139279.78481.62
420931-2093178.06579.92
521716-2171680.99382.94
621211-2121179.10981.07
30min121141-2114178.84880.452.6381.4983.112.64
220779-2077977.49880.05
321742-2174281.09083.72
421437-2143779.95282.59
522327-2232783.27286.03
621991-2199182.01884.77
45min119511-1951172.76977.664.3776.2081.124.28
220143-2014375.12678.45
320837-2083777.71481.16
420834-2083477.70381.14
521677-2167780.84784.44
621927-2192781.78085.35
60min120172-2017275.23478.223.6279.3982.463.58
219943-1994374.38078.45
321010-2101078.36082.58
421365-2136579.68483.90
521820-2182081.38185.78
621522-2152280.26984.66
极限120609-2060976.86476.823.1881.7781.853.14
219850-1985074.03378.85
320436-2043676.21981.22
420024-2002474.68279.70
521067-2106778.57283.79
621600-2160080.56085.75
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