熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003696136996376553769437588373790.99
210.963607336136361040.13
单位质量响应值RSD%判断
3398.093294.162.20数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-01批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min131642-3164284.78780.813.5884.7980.813.58
230597-3059781.98781.99
329991-2999180.36380.36
430378-3037881.40081.40
529989-2998980.35780.36
628340-2834075.93975.94
10min135522-3552295.18493.051.6895.3293.181.68
234978-3497893.72693.86
334612-3461292.74592.88
434888-3488893.48593.62
534588-3458892.68192.81
633761-3376190.46590.59
15min135781-3578195.87895.500.2796.1895.800.28
235661-3566195.55695.85
335601-3560195.39595.68
435679-3567995.60495.90
535641-3564195.50295.79
635489-3548995.09595.37
20min135912-3591296.22995.910.2296.6996.360.22
235793-3579395.91096.36
335680-3568095.60796.05
435824-3582495.99396.44
535775-3577595.86196.31
635777-3577795.86796.30
30min135679-3567995.60495.800.2796.2296.410.26
235677-3567795.59996.21
335710-3571095.68796.29
435780-3578095.87596.49
535739-3573995.76596.37
635927-3592796.26996.86
45min136683-3668398.29496.221.0999.0796.991.08
235759-3575995.81996.59
335673-3567395.58896.35
435845-3584596.04996.82
535852-3585296.06896.83
635645-3564595.51396.27
60min135852-3585296.06895.770.3097.0196.700.30
235615-3561595.43396.36
335671-3567195.58396.51
435773-3577395.85696.79
535659-3565995.55196.48
635869-3586996.11397.03
极限135792-3579295.90795.660.2597.0196.750.25
235685-3568595.62096.71
335563-3556395.29396.38
435656-3565695.54396.63
535715-3571595.70196.79
635789-3578995.89996.97
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.004069640463404704043140380404880.31
210.963611236084360980.06
单位质量响应值RSD%判断
3680.733293.617.85数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-02批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min129225-2922575.35771.856.5875.3671.846.58
228898-2889874.51474.51
329712-2971276.61376.61
427548-2754871.03371.03
527039-2703969.72069.72
624758-2475863.83963.84
10min134794-3479489.71787.202.7589.8487.322.76
234175-3417588.12188.24
334656-3465689.36189.49
433536-3353686.47386.59
533462-3346286.28286.40
632292-3229283.26583.37
15min135715-3571592.09190.941.0292.3791.211.03
235569-3556991.71591.99
335288-3528890.99091.27
435172-3517290.69190.95
535176-3517690.70290.96
634691-3469189.45189.70
20min135825-3582592.37591.850.4792.8092.260.48
235723-3572392.11292.54
335643-3564391.90692.33
435595-3559591.78292.20
535603-3560391.80392.21
635334-3533491.10991.50
30min135953-3595392.70591.910.7993.2992.480.79
235848-3584892.43493.01
335330-3533091.09991.68
435267-3526790.93691.50
535719-3571992.10292.67
635740-3574092.15692.70
45min136398-3639893.85392.560.8994.5993.280.88
235554-3555491.67692.41
335769-3576992.23192.96
436149-3614993.21193.93
535828-3582892.38393.10
635683-3568392.00992.71
60min135983-3598392.78392.050.8493.6892.930.84
235847-3584792.43293.32
335796-3579692.30093.19
435136-3513690.59991.47
535794-3579492.29593.17
635644-3564491.90892.76
极限135439-3543991.38092.110.4292.4393.140.40
235800-3580092.31193.35
335697-3569792.04593.09
435795-3579592.29893.32
535756-3575692.19793.22
635847-3584792.43293.44
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003627836196361723621036152362020.14
210.963606136071360660.02
单位质量响应值RSD%判断
3291.093290.690.01数据可信
供试品溶液-03批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126130-2613071.17576.574.2971.1876.574.29
229006-2900679.00979.01
329573-2957380.55380.55
428006-2800676.28576.29
527560-2756075.07075.07
628395-2839577.34577.34
10min132608-3260888.82092.412.4088.9492.542.40
234391-3439193.67793.81
334979-3497995.27995.41
433813-3381392.10392.23
533547-3354791.37891.50
634212-3421293.18993.32
15min134535-3453594.06996.211.1494.3496.491.14
235432-3543296.51396.80
335599-3559996.96797.26
435561-3556196.86497.14
535295-3529596.13996.42
635507-3550796.71797.00
20min134865-3486594.96896.740.9795.3997.180.97
235612-3561297.00397.45
335716-3571697.28697.74
435773-3577397.44197.88
535424-3542496.49196.93
635706-3570697.25997.70
30min135636-3563697.06897.180.3397.6597.780.33
235827-3582797.58898.20
335628-3562897.04697.66
435572-3557296.89497.50
535579-3557996.91397.51
635814-3581497.55398.16
45min135352-3535296.29597.160.5997.0497.920.59
235916-3591697.83198.60
335545-3554596.82097.60
435820-3582097.56998.34
535599-3559996.96797.73
635784-3578497.47198.24
60min135493-3549396.67996.820.6297.5897.750.62
235606-3560696.98797.92
335557-3555796.85397.79
435764-3576497.41798.35
535145-3514595.73196.65
635705-3570597.25698.19
极限135209-3520995.90596.221.1996.9797.311.18
235414-3541496.46497.56
335172-3517295.80496.91
435677-3567797.18098.27
534648-3464894.37795.46
635821-3582197.57298.67
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003625336342362563628636210362690.14
210.963600036038360190.08
单位质量响应值RSD%判断
3297.183286.410.24数据可信
供试品溶液-04批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min128755-2875578.30472.627.8378.3072.627.83
226714-2671472.74672.75
327779-2777975.64675.65
428022-2802276.30876.31
525746-2574670.11070.11
622991-2299162.60862.61
10min134631-3463194.30591.083.8594.4491.203.85
233486-3348691.18791.31
334178-3417893.07293.20
434167-3416793.04293.17
533161-3316190.30290.42
631057-3105784.57384.68
15min135664-3566497.11895.951.6097.4196.231.61
235131-3513195.66795.94
335622-3562297.00497.28
435666-3566697.12497.41
535116-3511695.62695.89
634220-3422093.18693.43
20min135886-3588697.72397.200.8998.1797.630.90
235802-3580297.49497.93
335838-3583897.59298.03
435824-3582497.55498.00
535760-3576097.38097.81
635055-3505595.46095.86
30min136018-3601898.08297.860.2198.6998.450.22
236035-3603598.12898.72
335946-3594697.88698.49
435877-3587797.69898.30
535876-3587697.69598.28
635867-3586797.67198.23
45min135910-3591097.78897.970.2698.5698.730.27
236094-3609498.28999.05
336091-3609198.28199.05
435963-3596397.93298.70
535895-3589597.74798.50
635912-3591297.79498.52
60min135850-3585097.62597.620.3598.5698.540.37
235921-3592197.81898.74
335912-3591297.79498.73
435933-3593397.85198.78
535862-3586297.65798.57
635602-3560296.94997.83
极限135771-3577197.41097.580.4398.5198.660.43
236026-3602698.10499.19
335607-3560796.96398.06
435974-3597497.96299.06
535847-3584797.61798.69
635767-3576797.39998.45
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