熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003612936361363313612336342362570.34
2 10.963617536428363020.50
单位质量响应值RSD%判断
3296.093312.230.35数据可信
加速3月-供试品溶液-25101501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min16903-690318.72821.427.9818.7321.427.98
28341-834122.62922.63
37662-766220.78720.79
48221-822122.30322.30
58639-863923.43723.44
67601-760120.62120.62
10min110860-1086029.46333.357.9429.4933.397.94
212789-1278934.69634.73
311485-1148531.15831.19
412836-1283634.82434.86
513522-1352236.68536.72
612273-1227333.29633.33
15min114764-1476440.05444.667.2040.1344.757.20
216887-1688745.81445.91
315308-1530841.53041.62
417210-1721046.69046.79
517874-1787448.49148.59
616723-1672345.36945.46
20min117668-1766847.93353.607.0248.0853.777.02
220071-2007154.45254.62
318464-1846450.09250.25
420917-2091756.74756.92
521103-2110357.25257.43
620324-2032455.13855.30
30min121974-2197459.61565.446.8759.8465.706.87
224278-2427865.86566.13
322166-2216660.13560.37
425413-2541368.94469.21
525560-2556069.34369.62
625346-2534668.76369.02
45min126975-2697573.18277.715.8873.5178.075.89
228764-2876478.03678.41
326198-2619871.07471.41
429954-2995481.26481.65
530179-3017981.87482.27
629786-2978680.80881.18
60min130027-3002781.46285.364.7081.9185.864.71
231761-3176186.16686.67
329252-2925279.36079.82
432555-3255588.32088.84
532353-3235387.77288.30
632837-3283789.08689.59
极限135729-3572996.93196.861.3297.5297.501.34
235607-3560796.60097.25
334869-3486994.59895.19
435757-3575797.00797.67
536005-3600597.68098.35
636256-3625698.36199.02
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003672236679365833637236384365480.45
2 10.963675136557366540.38
单位质量响应值RSD%判断
3322.553344.340.47数据可信
加速3月-供试品溶液-25101501批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115583-1558341.90539.869.0041.9039.869.00
215494-1549441.66641.67
312669-1266934.06934.07
416387-1638744.06744.07
513947-1394737.50537.51
614859-1485939.95839.96
10min123308-2330862.67861.826.1662.7561.896.15
221483-2148357.77157.84
321546-2154657.94058.00
425242-2524267.87967.95
522737-2273761.14361.21
623628-2362863.53963.61
15min129227-2922778.59577.923.9478.7778.093.95
228584-2858476.86677.03
327216-2721673.18873.34
430746-3074682.68082.87
528868-2886877.63077.79
629215-2921578.56378.74
20min133201-3320189.28287.833.9089.5988.133.90
232385-3238587.08887.38
330328-3032881.55681.83
434083-3408391.65491.98
532860-3286088.36588.66
633115-3311589.05189.35
30min135103-3510394.39794.244.3194.8594.684.32
234433-3443392.59593.03
332701-3270187.93888.35
437210-37210100.063100.54
534875-3487593.78494.22
635947-3594796.66697.12
45min135958-3595896.69696.353.5697.3196.953.57
235275-3527594.85995.45
333979-3397991.37491.93
437904-37904101.929102.57
535775-3577596.20496.80
636082-3608297.03097.64
60min136252-3625297.48797.023.6598.2697.783.65
235464-3546495.36896.12
334415-3441592.54793.26
438258-38258102.881103.69
535445-3544595.31796.07
636629-3662998.50099.28
极限136427-3642797.95797.193.1698.8998.123.17
235356-3535695.07795.99
334816-3481693.62594.49
438014-38014102.225103.21
535592-3559295.71296.63
636645-3664598.54499.48
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