熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003567935797358503572635214356530.72
210.963601135854359320.31
单位质量响应值RSD%判断
3241.183278.470.81数据可信
供试品溶液-05批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min128994-2899479.73274.156.4179.7374.156.41
227730-2773076.25676.26
327031-2703174.33374.33
426665-2666573.32773.33
527528-2752875.70075.70
623836-2383665.54765.55
10min134637-3463795.24992.283.6995.3892.403.70
234198-3419894.04294.17
333888-3388893.19093.31
433787-3378792.91293.03
533706-3370692.68992.82
631128-3112885.60085.71
15min135654-3565498.04696.801.3198.3497.081.32
235346-3534697.19997.48
335180-3518096.74397.02
435355-3535597.22497.50
535353-3535397.21897.50
634321-3432194.38094.63
20min136384-36384100.05397.741.74100.5198.171.75
235722-3572298.23398.68
335702-3570298.17898.62
435697-3569798.16498.60
535189-3518996.76797.21
634552-3455295.01695.42
30min135939-3593998.83097.750.7899.4598.350.79
235804-3580498.45999.07
335448-3544897.48098.08
435194-3519496.78197.38
535523-3552397.68698.29
635377-3537797.28497.85
45min136004-3600499.00998.670.6899.8099.430.68
235790-3579098.42099.19
335952-3595298.86699.63
435510-3551097.65098.41
536227-3622799.622100.39
635793-3579398.42899.16
60min135854-3585498.59697.620.9099.5598.550.92
235611-3561197.92898.87
335620-3562097.95398.88
435355-3535597.22498.15
535618-3561897.94798.88
634932-3493296.06196.95
极限135482-3548297.57397.821.2798.6998.911.25
235278-3527897.01298.11
335796-3579698.43799.53
435405-3540597.36198.45
535105-3510596.53697.63
636365-36365100.001101.06
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003640436622364513658836286364700.38
210.963664636382365140.52
单位质量响应值RSD%判断
3315.453331.570.35数据可信
供试品溶液-06批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127652-2765274.58266.017.6474.5866.017.63
222528-2252860.76260.76
322864-2286461.66861.67
424291-2429165.51765.52
525373-2537368.43568.44
624131-2413165.08565.09
10min133029-3302989.08587.723.0989.2187.833.09
230938-3093883.44583.55
332067-3206786.49086.59
433451-3345190.22390.33
533539-3353990.46090.57
632120-3212086.63386.74
15min135140-3514094.77892.782.9795.0593.032.97
232938-3293888.83989.08
333286-3328689.77890.02
435091-3509194.64694.91
535235-3523595.03595.30
634699-3469993.58993.84
20min135824-3582496.62395.471.8697.0595.871.87
234661-3466193.48693.87
334480-3448092.99893.39
436048-3604897.22797.64
535774-3577496.48896.91
635584-3558495.97696.38
30min135602-3560296.02495.900.6696.6296.470.67
235600-3560096.01996.56
335139-3513994.77695.33
435660-3566096.18196.76
535844-3584496.67797.26
635495-3549595.73696.30
45min135437-3543795.57995.961.0696.3396.701.06
235901-3590196.83197.54
335256-3525695.09195.80
435826-3582696.62997.37
535984-3598497.05597.80
635075-3507594.60395.33
60min135635-3563596.11396.130.5897.0297.020.58
235861-3586196.72397.59
335378-3537895.42096.29
435886-3588696.79097.69
535629-3562996.09797.00
635453-3545395.62396.51
极限135477-3547795.68796.101.0496.7697.151.03
236078-3607897.30898.34
335015-3501594.44195.47
435894-3589496.81297.87
535671-3567196.21097.28
635635-3563596.11397.16
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003620636214360943605636526362190.52
210.963635036150362500.40
单位质量响应值RSD%判断
3292.643307.480.32数据可信
供试品溶液-6011601批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min130889-3088983.90579.634.7683.9079.634.76
230098-3009881.75681.76
329549-2954980.26580.26
427157-2715773.76773.77
530059-3005981.65081.65
628141-2814176.44076.44
10min135495-3549596.41694.982.2596.5695.112.25
235514-3551496.46896.60
334962-3496294.96895.10
433533-3353391.08791.21
535582-3558296.65296.79
634707-3470794.27694.40
15min136339-3633998.70997.641.2199.0197.931.21
235873-3587397.44397.74
335653-3565396.84597.14
435441-3544196.26996.54
536585-3658599.37799.67
635784-3578497.20197.49
20min136272-3627298.52797.860.4498.9998.320.45
235998-3599897.78298.24
335983-3598397.74298.20
435881-3588197.46597.90
536151-3615198.19898.66
635877-3587797.45497.90
30min136061-3606197.95497.870.5298.5898.490.52
236023-3602397.85098.47
335675-3567596.90597.52
436071-3607197.98198.58
536169-3616998.24798.87
636186-3618698.29398.90
45min135762-3576297.14197.600.5997.9398.380.58
235667-3566796.88397.67
336088-3608898.02798.80
435883-3588397.47098.23
536234-3623498.42399.21
635954-3595497.66398.44
60min136157-3615798.21497.550.4499.1798.490.44
235694-3569496.95797.90
335853-3585397.38998.33
435855-3585597.39498.32
535999-3599997.78598.74
635908-3590897.53898.47
极限135908-3590897.53897.340.8098.6698.440.80
235497-3549796.42297.53
335768-3576897.15898.26
435683-3568396.92798.01
536341-3634198.71499.83
635803-3580397.25398.35
熊去氧胆酸颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号110755-202306对照品来源自制对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.003648136366364723650836721365100.36
210.963656036774366670.42
单位质量响应值RSD%判断
3319.093345.530.57数据可信
供试品溶液-6011602批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min127827-2782774.85769.585.2674.8669.585.26
226504-2650471.29871.30
324511-2451165.93665.94
426573-2657371.48371.48
525496-2549668.58668.59
624282-2428265.32065.32
10min133594-3359490.37088.232.8990.4988.352.89
233790-3379090.89791.02
333117-3311789.08789.20
432388-3238887.12687.25
532720-3272088.01988.13
631188-3118883.89884.01
15min135774-3577496.23494.171.6496.5194.431.65
235337-3533795.05995.33
334999-3499994.15094.41
435069-3506994.33894.60
534800-3480093.61493.88
634057-3405791.61691.86
20min135859-3585996.46395.350.6296.9095.780.63
235443-3544395.34495.77
335283-3528394.91495.33
435321-3532195.01695.44
535490-3549095.47195.89
635283-3528394.91495.32
30min135962-3596296.74096.080.3897.3496.660.38
235585-3558595.72696.31
335706-3570696.05296.63
435648-3564895.89696.48
535641-3564195.87796.45
635752-3575296.17596.73
45min135836-3583696.40195.490.8797.1696.230.87
235088-3508894.38995.14
335176-3517694.62695.36
435788-3578896.27297.01
535527-3552795.57096.31
635568-3556895.68096.40
60min135817-3581796.35096.110.4597.2797.010.45
235980-3598096.78997.69
335570-3557095.68696.58
435571-3557195.68896.59
535755-3575596.18397.08
635682-3568295.98796.87
极限135748-3574896.16596.000.5997.2497.060.58
235818-3581896.35397.42
335341-3534195.07096.12
435905-3590596.58797.65
535545-3554595.61896.67
635766-3576696.21397.25
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