辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.422734762718742732272716932722892725120.30
210.302721742714152717940.20
单位质量响应值RSD%判断
26152.7826387.770.64数据可信
长期6月-供试品溶液-2025071921批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1183433-18343369.68771.201.4269.6971.201.41
2187322-18732271.16471.16
3190603-19060372.41172.41
4187060-18706071.06571.06
5185987-18598770.65770.66
6190013-19001372.18772.19
10min1211016-21101680.16681.791.3280.3882.001.31
2217560-21756082.65282.87
3219127-21912783.24783.46
4215008-21500881.68381.90
5214114-21411481.34381.55
6214873-21487381.63181.85
15min1224289-22428985.20886.371.2385.6686.821.22
2231211-23121187.83888.30
3229384-22938487.14487.61
4228436-22843686.78487.24
5224705-22470585.36685.82
6225984-22598485.85286.31
20min1230142-23014287.43289.471.8188.1490.181.80
2241710-24171091.82792.55
3238820-23882090.72991.46
4236092-23609289.69290.41
5233328-23332888.64289.35
6232892-23289288.47789.20
30min1235131-23513189.32790.651.7790.2991.641.76
2246022-24602293.46594.47
3240528-24052891.37892.38
4237154-23715490.09691.08
5238164-23816490.48091.46
6234641-23464189.14190.13
45min1235322-23532289.40091.011.5390.6492.271.52
2244274-24427492.80194.08
3243506-24350692.50993.78
4238125-23812590.46591.72
5239587-23958791.02092.27
6236588-23658889.88191.13
60min1234735-23473589.17790.841.6490.6892.371.63
2244951-24495193.05894.62
3242135-24213591.98893.54
4239253-23925390.89392.42
5238024-23802490.42691.95
6235590-23559089.50291.02
极限1261996-26199699.533100.631.08101.30102.431.08
2269222-269222102.279104.12
3265111-265111100.717102.55
4264907-264907100.639102.44
5266443-266443101.223103.02
6261594-26159499.381101.17
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.422711052721342713702717752711172715000.17
210.302699152711272705210.32
单位质量响应值RSD%判断
26055.6626264.170.57数据可信
长期6月-供试品溶液-2025071921批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1187343-18734371.47274.332.8371.4774.332.83
2193235-19323573.72073.72
3194166-19416674.07574.08
4193292-19329273.74273.74
5196960-19696075.14175.14
6204068-20406877.85377.85
10min1213339-21333981.39083.211.9081.6083.431.91
2219689-21968983.81384.03
3215963-21596382.39182.61
4214318-21431881.76481.98
5222365-22236584.83485.06
6222938-22293885.05285.29
15min1226234-22623486.31087.111.4486.7787.591.45
2229238-22923887.45687.93
3225615-22561586.07386.54
4224851-22485185.78286.25
5232970-23297088.87989.36
6231128-23112888.17788.67
20min1232804-23280488.81689.900.9289.5390.630.93
2236554-23655490.24790.98
3233826-23382689.20689.93
4234858-23485889.60090.32
5238138-23813890.85191.60
6237692-23769290.68191.43
30min1235478-23547889.83690.390.9690.8291.390.96
2239049-23904991.19992.20
3234018-23401889.27990.27
4236216-23621690.11891.11
5240066-24006691.58792.61
6236755-23675590.32391.35
45min1236351-23635190.16990.781.1191.4292.061.10
2239877-23987791.51492.79
3235760-23576089.94491.21
4236257-23625790.13391.40
5242385-24238592.47193.77
6237093-23709390.45291.75
60min1236979-23697990.40990.960.9691.9392.510.96
2241318-24131892.06493.62
3236155-23615590.09491.63
4236513-23651390.23191.76
5240977-24097791.93493.51
6238680-23868091.05892.63
极限1261678-26167899.832101.121.16101.63102.941.14
2268037-268037102.258104.09
3265024-265024101.108102.91
4268714-268714102.516104.32
5265500-265500101.290103.14
6261432-26143299.738101.58
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