枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064455954458104462204451284454944456490.10
213.134452804450294451540.04
单位质量响应值RSD%判断
34123.2033903.580.46数据可信
供试品溶液-2026010311批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1241171-24117144.87850.1810.4244.8850.1810.42
2256907-25690747.80747.81
3297073-29707355.28155.28
4300784-30078455.97155.97
5237552-23755244.20544.20
6284414-28441452.92552.93
5min1360131-36013167.01565.152.9867.0265.152.98
2354386-35438665.94665.95
3346602-34660264.49864.50
4361988-36198867.36167.36
5336251-33625162.57162.57
6341222-34122263.49663.50
10min1350817-35081765.28263.362.7565.2863.362.75
2344358-34435864.08064.08
3338196-33819662.93362.93
4347377-34737764.64264.64
5337702-33770262.84162.84
6324506-32450660.38660.39
15min1337908-33790862.88061.641.9962.8861.641.99
2334435-33443562.23362.23
3328306-32830661.09361.09
4334551-33455162.25562.26
5332923-33292361.95261.95
6319473-31947359.44959.45
30min1306818-30681857.09457.011.6157.0957.001.61
2308828-30882857.46857.47
3309165-30916557.53157.53
4312398-31239858.13358.13
5300510-30051055.92055.92
6300333-30033355.88855.89
45min1289715-28971553.91253.341.6353.9153.341.64
2288083-28808353.60853.61
3286524-28652453.31853.32
4290623-29062354.08154.08
5287406-28740653.48253.48
6277635-27763551.66451.66
极限1271342-27134250.49349.872.6650.4949.872.66
2270271-27027150.29350.29
3269761-26976150.19950.20
4275400-27540051.24851.25
5266413-26641349.57649.58
6254713-25471347.39847.40
枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064523444534374528904533364483194520650.48
213.134498404494814496600.06
单位质量响应值RSD%判断
34614.4734246.760.76数据可信
供试品溶液-2026010311批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1259891-25989147.77749.768.4747.7849.768.47
2249103-24910345.79445.79
3255229-25522946.92046.92
4260360-26036047.86347.86
5300259-30025955.19855.20
6299324-29932455.02655.03
5min1364389-36438966.98765.641.4366.9965.641.43
2361090-36109066.38066.38
3352683-35268364.83564.84
4354293-35429365.13165.13
5358354-35835465.87865.88
6351519-35151964.62164.62
10min1345733-34573363.55762.312.1263.5662.312.12
2343135-34313563.08063.08
3336990-33699061.95061.95
4334630-33463061.51661.52
5327621-32762160.22860.23
6345501-34550163.51563.51
15min1324589-32458959.67060.332.7359.6760.322.73
2324600-32460059.67259.67
3328640-32864060.41560.42
4341357-34135762.75362.75
5334269-33426961.45061.45
6315466-31546657.99357.99
30min1306454-30645456.33756.500.9556.3456.500.95
2310405-31040557.06357.06
3304852-30485256.04256.04
4309980-30998056.98556.98
5309000-30900056.80556.80
6303321-30332155.76155.76
45min1288122-28812252.96753.420.6952.9753.420.69
2289324-28932453.18753.19
3288934-28893453.11653.12
4292443-29244353.76153.76
5292484-29248453.76853.77
6292114-29211453.70053.70
极限1274287-27428750.42349.721.4050.4249.721.40
2272433-27243350.08250.08
3272618-27261850.11650.12
4271966-27196649.99750.00
5266972-26697249.07849.08
6264623-26462348.64748.65
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