替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.312835728374283182845128309283620.20
214.232850028649285740.37
单位质量响应值RSD%判断
1981.972008.010.93数据可信
供试品溶液-6013101批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124553-2455388.66390.081.5488.6690.081.54
225328-2532891.46291.46
324809-2480989.58889.59
425008-2500890.30690.31
525442-2544291.87391.87
624535-2453588.59888.60
10min125976-2597693.80295.851.6794.6996.741.66
226996-2699697.48598.40
326302-2630294.97995.87
426565-2656595.92996.83
527115-2711597.91598.83
626297-2629794.96195.85
15min125883-2588393.46695.041.4095.2996.901.39
226662-2666296.27998.17
325987-2598793.84195.69
426207-2620794.63696.50
526804-2680496.79298.69
626377-2637795.25097.09
20min125757-2575793.01193.821.4095.7796.631.39
226623-2662396.13898.99
325551-2555192.26795.05
425936-2593693.65796.47
526049-2604994.06596.93
625971-2597193.78496.57
30min125790-2579093.13092.931.0396.8296.681.03
226133-2613394.36998.18
325514-2551492.13395.84
425709-2570992.83896.58
525872-2587293.42697.23
625393-2539391.69695.42
极限125218-2521891.06590.791.3295.6995.471.27
225151-2515190.82395.58
324638-2463888.97093.60
425669-2566992.69397.37
525065-2506590.51295.25
625111-2511190.67895.32
替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.312818628016281112791727934280330.42
214.232823028194282120.10
单位质量响应值RSD%判断
1958.981982.570.85数据可信
供试品溶液-6013101批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122859-2285983.56085.801.5283.5685.801.53
223898-2389887.35887.36
323366-2336685.41385.41
423717-2371786.69686.70
523443-2344385.69485.69
623555-2355586.10486.10
10min124592-2459289.89591.431.5890.7392.281.58
225706-2570693.96794.84
324867-2486790.90091.75
425174-2517492.02292.89
524978-2497891.30692.16
624752-2475290.47991.34
15min124418-2441889.25890.021.5290.9991.791.50
224638-2463890.06391.88
324088-2408888.05289.82
424800-2480090.65592.44
525202-2520292.12493.89
624605-2460589.94291.71
20min124380-2438089.12088.392.2491.7591.072.19
224965-2496591.25893.97
323443-2344385.69488.34
424497-2449789.54792.24
523961-2396187.58890.28
623843-2384387.15789.82
30min123590-2359086.23287.701.5289.7591.261.49
223965-2396587.60391.23
323567-2356786.14889.65
424445-2444589.35792.95
524313-2431388.87592.44
624069-2406987.98391.52
极限124111-2411188.13688.751.9692.5293.181.91
224720-2472090.36294.86
323839-2383987.14291.50
424919-2491991.09095.57
524351-2435189.01493.47
623739-2373986.77691.19
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