枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064471054461284472304448484460284462680.22
213.134470474483474476970.21
单位质量响应值RSD%判断
34170.6034097.260.16数据可信
供试品溶液-2026010411批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1284396-28439652.73548.2213.4252.7348.2213.43
2264275-26427549.00449.00
3278263-27826351.59751.60
4191692-19169235.54535.54
5281760-28176052.24652.25
6259961-25996148.20448.20
5min1353718-35371865.58964.573.7665.5964.573.75
2357198-35719866.23466.23
3356220-35622066.05366.05
4347974-34797464.52464.52
5351848-35184865.24265.24
6322434-32243459.78859.79
10min1346750-34675064.29763.193.5664.3063.193.57
2345999-34599964.15764.16
3349084-34908464.72964.73
4348602-34860264.64064.64
5336203-33620362.34162.34
6317938-31793858.95458.95
15min1333454-33345461.83160.654.3361.8360.654.33
2330110-33011061.21161.21
3334685-33468562.05962.06
4329613-32961361.11961.12
5335973-33597362.29862.30
6298676-29867655.38255.38
30min1313635-31363558.15655.753.6958.1655.753.69
2306421-30642156.81956.82
3307508-30750857.02057.02
4298850-29885055.41555.41
5295074-29507454.71554.71
6282503-28250352.38452.38
45min1289520-28952053.68552.332.3953.6852.332.39
2284055-28405552.67152.67
3286254-28625453.07953.08
4275977-27597751.17351.17
5285467-28546752.93352.93
6272042-27204250.44450.44
极限1261959-26195948.57449.301.6848.5749.301.68
2268337-26833749.75749.76
3270022-27002250.06950.07
4266411-26641149.40049.40
5269505-26950549.97349.97
6259010-25901048.02748.03
枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064421094476254456374465104467314457220.49
213.134534714501674518190.52
单位质量响应值RSD%判断
34128.7934411.200.59数据可信
供试品溶液-2026010411批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1283241-28324152.31350.5510.5352.3150.5510.53
2269817-26981749.83349.83
3277544-27754451.26051.26
4218931-21893140.43540.44
5294227-29422754.34254.34
6298341-29834155.10255.10
5min1348691-34869164.40162.562.5964.4062.562.59
2345871-34587163.88063.88
3338925-33892562.59762.60
4323613-32361359.76959.77
5338622-33862262.54162.54
6336769-33676962.19962.20
10min1340040-34004062.80361.741.3262.8061.741.32
2337342-33734262.30562.30
3336074-33607462.07162.07
4330684-33068461.07561.08
5328123-32812360.60260.60
6333585-33358561.61161.61
15min1330987-33098761.13159.901.7661.1359.901.75
2328997-32899760.76360.76
3326507-32650760.30460.30
4320023-32002359.10659.11
5315908-31590858.34658.35
6323391-32339159.72859.73
30min1302710-30271055.90855.061.0655.9155.071.06
2298052-29805255.04855.05
3297775-29777554.99755.00
4300528-30052855.50555.51
5294087-29408754.31654.32
6295701-29570154.61454.61
45min1282191-28219152.11952.050.5352.1252.050.53
2280350-28035051.77951.78
3280016-28001651.71751.72
4284105-28410552.47252.47
5282398-28239852.15752.16
6281722-28172252.03252.03
极限1268838-26883849.65349.240.7649.6549.240.75
2266528-26652849.22649.23
3265083-26508348.95948.96
4267960-26796049.49049.49
5267659-26765949.43549.43
6263478-26347848.66348.66
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