枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064466574472274471234461174466094467470.10
213.134462034477934469980.26
单位质量响应值RSD%判断
34207.2734044.020.34数据可信
供试品溶液-2026010511批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1295206-29520654.75348.0311.4454.7548.0311.44
2277933-27793351.54951.55
3266246-26624649.38149.38
4223261-22326141.40941.41
5268205-26820549.74549.74
6222909-22290941.34341.34
5min1343371-34337163.68662.004.3863.6962.004.38
2346455-34645564.25864.26
3347385-34738564.43064.43
4324119-32411960.11560.12
5333728-33372861.89761.90
6310524-31052457.59457.59
10min1327106-32710660.66959.263.7660.6759.263.76
2329279-32927961.07261.07
3329819-32981961.17261.17
4320705-32070559.48259.48
5300309-30030955.69955.70
6309974-30997457.49257.49
15min1311532-31153257.78157.663.3057.7857.663.29
2302689-30268956.14056.14
3325993-32599360.46360.46
4319988-31998859.34959.35
5303801-30380156.34756.35
6301179-30117955.86055.86
30min1290865-29086553.94754.681.4053.9554.681.40
2300927-30092755.81455.81
3293931-29393154.51654.52
4298775-29877555.41455.41
5292658-29265854.28054.28
6291606-29160654.08554.08
45min1277758-27775851.51651.282.1251.5251.282.12
2280727-28072752.06752.07
3275851-27585151.16351.16
4284635-28463552.79252.79
5270215-27021550.11750.12
6269751-26975150.03150.03
极限1260569-26056948.32848.663.9548.3348.663.95
2277325-27732551.43651.44
3259694-25969448.16648.17
4269426-26942649.97149.97
5260477-26047748.31148.31
6246608-24660845.73945.74
枸橼酸西地那非口崩片项目信息
介质体积(ml)900取样体积(ml)0补液体积(ml)0
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.064438544474044464574468774477244464630.35
213.134480884480484480680.01
单位质量响应值RSD%判断
34185.5334125.510.13数据可信
供试品溶液-2026010511批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
2min1291932-29193254.09853.748.3154.1053.748.31
2285363-28536352.88052.88
3286139-28613953.02453.02
4335363-33536362.14662.15
5265765-26576549.24949.25
6275317-27531751.01951.02
5min1341802-34180263.33966.062.5863.3466.062.58
2357520-35752066.25266.25
3358230-35823066.38366.38
4369704-36970468.51068.51
5352236-35223665.27365.27
6359370-35937066.59566.59
10min1341605-34160563.30361.424.5963.3061.424.59
2348681-34868164.61464.61
3339554-33955462.92262.92
4325083-32508360.24160.24
5306246-30624656.75056.75
6327501-32750160.68960.69
15min1312972-31297257.99761.023.4658.0061.023.46
2333706-33370661.83961.84
3335800-33580062.22762.23
4345321-34532163.99163.99
5325114-32511460.24760.25
6322651-32265159.79059.79
30min1299480-29948055.49656.120.6555.5056.120.65
2303253-30325356.19656.20
3302530-30253056.06256.06
4305518-30551856.61556.62
5303448-30344856.23256.23
6302819-30281956.11556.12
45min1280313-28031351.94552.460.9251.9452.460.92
2280944-28094452.06152.06
3283310-28331052.50052.50
4286111-28611153.01953.02
5281700-28170052.20252.20
6286248-28624853.04453.04
极限1266444-26644449.37549.170.9849.3749.170.98
2263930-26393048.90948.91
3268472-26847249.75049.75
4267229-26722949.52049.52
5264564-26456449.02649.03
6261286-26128648.41948.42
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